Technical data sheet recording instrument parameters and calibration details for GCMS Method 508 analysis conducted in November 2001.
NYC-WTC_000033886–000033901Folder label: “GCMS X 11/20/01 A 11/26/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\NOV2601\LBA.D Vial: 9 Acq On : 26 Nov 2001 6:31 pm Operator: 209 GALOS Sample : 11/20 lab bik scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Ethanedioic acid, bis(trimethy Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
39.60 2.07 ug/1 401611 Perylene-dl2 37.12
Hit# of 5 Tentative, ID MW MolForm CAS# Qual
1 Ethanedioic acid, bis(trimethylsily 234 C8H18O4Si2 018294-04-7 27 2 3,6-Dioxa-2,4,5,7-tetrasilaoctane, 294 C10H3002Si4 004342-25-0 25 3 3-Isopropoxy-1,1,1, 7,7,7-hexamethyl 576 C18H5207Si7 071579-69-6 25 4 Mercaptoacetic acid, bis(trimethyls 236 C8H2002SSi2 00 6 398-62 - 5 2 3 Abundance 73 Scan 3764 (39.596 min): LBA.D (-) m/z 73.00 100.00% 147
221 5000 281 355 . 1 429 39.20 39.40 39.60 39.80 40.00 40 . 4103.+ —191T — —.T253,r 132714 014— TT m/z 146.95 78.49% miz-> 50 100 150.. 200 _ 250 300 350 _ 400 450 500 550 . Abundance #71006: Ethanedioic acid, bis(trimethylsiiyl) ester 73 147 5000 " 1 - Trer 39.20 39.40 39.60 39.80 40.00 ! 45 m/z 221.05 52.33% I I 117 190 219 ............................ ’ ' i ' ‘ ' TT. ’'. TTT ' miz-> 50 100 150 200 ' 250 300 350 400 ' 450 ' 500 550 ' Abundance #41682: 3.6-0022-24,5 7-tetrasilaoctane, 2,2.4,4.5.5.7.7- 147 221
73 39.20 39.40 39.60 39.80 40.00 5000 m/z 281.0 28.23% 191 117 279 —............ — TT—rrruuur TT TTTr n r j i i i i । i i m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #60503: 3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim T T T T 73 39.20 39.40 39.60 39.80 40.00 m/z 207.00 26.82% 5000 147
m/z-> 50 100 150 200 241 2 827 . ... . 581 250 300 350 400 ' 450 500 550 T T T T 39.20 39.40 39.60 39.80 40.00
LBA.D GCMS1126.M Thu Jan 03 12:52:28 2002 Page 6
NYC-WTC_000033897
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NYC-WTC_000033707
Laboratory report of a GCMS blank analysis for sample AD28143 conducted on November 28, 2001, listing various organic compounds below detection limits.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
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Header page for a gas chromatography-mass spectrometry scan file related to environmental testing at the World Trade Center site.
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Analytical commentary for sample AD28157 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033765
Analytical commentary for sample AD28149 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017663
Laboratory report documenting gas chromatography-mass spectrometry blank analysis conducted on December 27, 2001.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019049
Laboratory report documenting gas chromatography-mass spectrometry blank analysis for volatile organic compounds conducted on January 7, 2002.
1 shared topics · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034180
Laboratory report detailing GCMS analysis of sample AD28269 conducted on November 30, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034331
Laboratory report documenting GCMS analysis of sample AD28427 conducted between November 21 and 26, 2001.
1 shared non-person entities · 1 shared topics · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018420
Laboratory report documenting GCMS blank analysis of sample AD30643 conducted on February 1, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000047955
GCMS blank analysis report for sample AE08209 listing volatile organic compounds from April 2002.
1 shared topics · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034958
Calibration report showing recovery percentages for various chemical standards used in the GCMS analysis.
1 shared non-person entities · 1 shared topics · similarity 0.991
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000034830
Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28666 analyzed in early December 2001.
1 shared non-person entities · 1 shared topics · similarity 0.991
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NYC-WTC_000033704
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
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NYC-WTC_000033705
Fragmented page from a GCMS-related record dated between November 20 and 26, 2001, likely part of the WTC environmental monitoring series.
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NYC-WTC_000033707
Laboratory report of a GCMS blank analysis for sample AD28143 conducted on November 28, 2001, listing various organic compounds below detection limits.
Filed in the same folder
NYC-WTC_000033723
Calibration record for GCMS instrument 209 using method GCMS1126, dated November 26-28, 2001, listing standard compounds and retention times.
Filed in the same folder
NYC-WTC_000033726
Laboratory report of a GCMS reference analysis for sample AD28143 conducted on November 28, 2001, listing detected compounds and retention times.
Filed in the same folder