GCMS reference analysis results for sample AD28143, Nov 2001

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\NOV2601\REF.D Vial: 22 Acq On : 27 Nov 2001 7:14 am Operator: 209 GALOS Sample : 11/20 scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Nov 28 15:15 2001 Quant Results File: GCMS1126.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Nov 27 12:20:14 2001 Response via : Initial Calibration DataAcq Meth : NP103001

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.69 152 737564 20.00 ug/1 0.00 15) Naphthalene-d8 15.30 136 2771521 20.00 ug/1 0.00 26) Acenaphthene-diO 20.57 164 1336543 20.00 ug/1 0.00 4 2) Phenanthrene-dl0 25.00 188 1803858 20.00 ug/1 0.00 53) Chrysene-dl2 33.03 240 905649 20.00 ug/1 0.00 59) Perylene-dl2 37.11 264 597398 20.00 ug/1 0.00

System Monitoring Compounds 52) 2,4-DDD 30.07 235 114097 5.31 ug/mL 0.00 Spiked Amount 5.000 Recovery = 106.20%

Target Compounds AU- Qvalue 2 )—Pyr idine 0.00 79 0 N.D. 3) N-nitroso-dimethyl amine 5.44 74 69578 2.14 ug/1 94 4)—Phenel 11.12 94 5312 N.D. 5) bis(2-Chloroethyl)ether 11.12 93 182135 3.58 ug/1 99 6) -2-Chlorophenol. 0.00 128 0 N.D. 7) 1,3-Dichlorobenzene 11.59 146 126156 2.35 ug/1 98 8) 1,4-Dichlorobenzene 11.74 146 137442m 2.53 ug/1 9) 1,2-Dichlorobenzene 12.25 146 141571 2.83 ug/1 97 10) 2-Methylphenol 12.26 108 1074 N.D. 11) 2,2'-oxybis(1-Chloropropan 12.59 45 256885 3.96 ug/1 94 12) 3&4-Methylphenol 13 .36 108 250 N.D. 13) N-Nitroso-di-n-propylamine 12.98 70 103184 3.56 ug/1 97 14) Hexachloroethane 13.08 117 35716 1.81 ug/1 85 16) Nitrobenzene 13.37 77 142327 3.29 ug/1 96 17) Isophorone 14.02 82 315163 3.79 ug/1 97 18) -2-Nitrophenel- 14.02 139 5824 N.D. 19) 2,4 Dimethylphenol 14.02 107 455 N.D. 20) bis(2-Chloroethoxy)methane 14.70 93 214430 3.84 ug/1 98 21) -2,4-Dichl erophenol 0.00 162 0 N.D. 22) 1,2,4-Trichlorobenzene 15.19 180 116568 2.90 ug/1 99 23) Naphthalene 15.36 128 491752 3.71 ug/1 99 24) Hexachlorobutadiene 15.91 225 37162 1.89 ug/1 97 25) -4Chlere-3 methylphenol 0.00 107 0 N.D. 27) Hexachlorocyclopentadiene 18.08 237 2428 0.25 ug/1 # 79 28) -2,4,6 Trichlorophenol 0.00 196 0 N.D. 29) 2,4,5-Trichlorophenol 0.00 196 0 N.D. 30) 2-Chloronaphthalene 18.85 162 268953 3.53 ug/1 98 31) Dimethylphthalate 19.95 163 340499 3.83 ug/1 100 32) 2,6-Dinitrotoluene 20.16 165 53744m 2.56 ug/1 (#) = qualifier out of range (m) = manual integration REF.D GCMS1126.M Wed NOV 28 15:16:16 2001 Page 1

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