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GCMS reference analysis results for sample AD28143, Nov 2001

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Laboratory report of a GCMS reference analysis for sample AD28143 conducted on November 28, 2001, listing detected compounds and retention times.

NYC-WTC_000033726–000033730

Folder label: “GCMS X 11/20/01 A 11/26/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) $ Data File : C:\HPCHEM\1\DATA\NOV2601\REF.D Vials 22 Acq On s 27 Nov 2001 7s14 am Operators 209 GALOS Sample s 11/20 scan Inst s GC/MS 209 Mise Multiplrs 1.00 MS Integration Params s RTEINT.P Quant Times Nov 28 15$15 2001 Quant Results Files GCMS1126.RES

Quant Method s C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title s 209 625/TCLP calibration table Last Update s Tue Nov 27 12:20:14 2001 Response via : Initial Calibration DataAcq Meth $ NP103001

Compound R.T. Qlon Response Cone Unit Qvalue

33) Acenaphthylene 20.10 152 399827 3.73 ug/1 100 34) Acenaphthene 20.66 153 300911 3.93 ug/1 100 35) -2,4—Dinitrophenol 0.00 184 0 N.D. 36) -4-Ni trophenol— 0.00 65 0 N.D. d 37) 2,4-Dinitrotoluene 21.32 165 60808 2.28 ug/1 # 88 38) Diethylphthalate 22.08 149 325101 3.96 ug/1 99 39) 4-Chlorophenyl-phenylether 22.21 204 144366 4.02 ug/1 98 40) Fluorene 22.18 166 311453 3.96 ug/1 97 41) Azobenzen/ 1,2-Diphenylhyd 22.67 77 296086 3.49 ug/L 97 43) 4, 6-Dinitro-2-methylphenol 0.00 198 0 N.D. 44) N-Nitrosodiphenylamine 22.61 168 110804 3.46 ug/1 100 45) 4-Bromophenyl-phenylether 23.67 248 69868 3.94 ug/1 99 46) Hexachlorobenzene 24.10 284 78141 4.00 ug/1 97 47) -Pentachlorophenel 0.00 266 0 N.D. 4 8) Phenanthrene 25.06 178 403833 4.23 ug/1 98 49) Anthracene 25.19 178 360821 3.79 ug/1 100 50) Di-n-butylphthalate 27.00 149 450705 3.55 ug/1 100 51) Fluoranthene 28.67 202 334319 3.63 ug/1 97 54) Pyrene 29.34 202 346545 4.43 ug/1 99 55) Butylbenzylphthalate 31.51 149 115349 2.83 ug/1 100 56) Benzo(a)anthracene 32.97 228 197805 3.67 ug/1 100 57) Bis(2-ethylhexyl)phthalate 33.30 149 151421 2.74 ug/1 99 58) Chrysene 33.09 228 233530 4.41 ug/1 99 60) Di-n-Octylphthalate 35.05 149 122926 1.55 ug/1 # 95 61) Benzo(b)fluoranthene 36.05 252 171535 3.82 ug/1 98 62) Benzo(k)fluoranthene 36.11 252 201066 4.36 ug/1 97 63) Benzo(a)pyrene 36.94 252 129268 3.31 ug/1 99 64) Indeno(l,2,3-cd)pyrene 40.80 276 132084 3.38 ug/1 96 65) Dibenz(a,h)anthracene 40.86 278 117038 3.83 ug/1 98 66) Benzo(g,h,i)perylene 41.89 276 128513 3.85 ug/1 98

(#) = qualifier out of range (m) = manual integration REF.D GCMS1126.M Wed Nov 28 15s16s19 2001 Page 2

NYC-WTC_000033729

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NYC-WTC_000033729Source: NYC Law Department, mirrored locally

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