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GCMS blank analysis results for sample AD28143, Nov 2001

Machine-extracted title · confidence 100%

Laboratory report of a GCMS blank analysis for sample AD28143 conducted on November 28, 2001, listing various organic compounds below detection limits.

NYC-WTC_000033707–000033722

Folder label: “GCMS X 11/20/01 A 11/26/01”

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\NOV2601\LBA.D Vial : 9 Acq On : 26 NOV 2001 6:31 pm Operator : 209 GALOS Sample : 11/20 lab bik scan Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 11.560 706 710 720 rVB 53361 129074 1.79% 0.349% 2 11.697 720 725 743 rBV 2072266 5101607 70.81% 13.780% 3 15.305 1112 1118 1136 rBV 3109673 6811636 94.54% 18.398% 4 20.575 1686 1692 1709 rBV 3376468 7204699 100.00% 19.460% 5 24.991 2167 2173 2186 IBV2 2955565 6615516 91.82% 17.869%

6 30.067 2721 2726 2733 rBV 270994 546992 7.59% 1.477% 7 33.023 3035 3048 3055 rBV2 1934876 4678604 64.94% 12.637% 8 33.308 3072 3079 3086 rBV 79137 176847 2.45% 0.478% 9 35.575 3320 3326 3335 rBV2 37014 115211 1.60% 0.311% 10 36.723 3445 3451 3468 rBV 48439 176851 2.45% 0.478%

11 37.118 3486 3494 3515 rBV2 1390224 3876036 53.80% 10.469% 12 37.999 3585 3590 3591 rBV 87030 85848 1.19% 0.232% 13 38.027 3591 3593 3613 rVB2 60967 219627 3.05% 0.593% 14 39.596 3754 3764 3784 rBV2 66667 401611 5.57% 1.085% 15 41.543 3964 3976 3988 rBV4 57392 383337 5.32% 1.035%

16 43.966 4226 4240 4260 rBV4 42864 365657 5.08% 0.988% 17 47.051 4562 4576 4578 rBV6 24570 133756 1.86% 0.361%

Sum of corrected areas: 37022909

LBA.D GCMS1126.M Tue NOV 27 12:44:05 2001

NYC-WTC_000033711

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NYC-WTC_000033711Source: NYC Law Department, mirrored locally

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GCMS comments for sample AD28157, Nov 2001 · Box DEP Box 21

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Analytical commentary for sample AD28157 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.

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GCMS comments for sample AD28149, Nov 2001 · Box DEP Box 21

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Analytical commentary for sample AD28149 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.

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