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GCMS analysis results for sample AD27771, Jan 2002

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Laboratory report documenting GCMS analysis of environmental sample AD27771 conducted on January 3, 2002.

NYC-WTC_000033580–000033592

Folder label: “GCMS X 11/19/01 A 12/19 - 12/20/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\DEC1901\27771.D Vial: 30 Acq On : 19 Dec 2001 7:33 pm Operator: 209 GALOS Sample : gc/msunknown 11/19 Inst • : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Jan 3 9:46 2002 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 14 12:19:30 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 3 3) Phenanthrene 24.98 178 929 / N.D. 34) Anthracene 24.98 178 929/ N.D. 35) Di-n-butylphthalate 27.02 149 2139 / N.D. 36) Fluoranthene 0.00 202 0 N.D. 3 9) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 / N.D. 41) Benzo(a)anthracene 33.01 228 3960 7 N.D. 42) Bis(2-ethylhexyl)phthalate 33.29 149 2667 4 N.D. 43) Chrysene 33.01 228 3960 / N.D. 45) Di-n-Octylphthalate 35.47 149 (103 : N.D. 46) Benzo(b)fluoranthene 0.00 252 0 N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. v 48) Benzo(a)pyrene 37.10 252 5036 / N.D. 49) Indeno(l,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 27771.D GCMS1126.M Thu Jan 03 09:46:55 2002 Page 2

NYC-WTC_000033583

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NYC-WTC_000033583Source: NYC Law Department, mirrored locally

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