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GCMS analysis results for sample AD27772, Jan 2002

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Laboratory report documenting GCMS analysis of environmental sample AD27772 conducted on January 3, 2002.

NYC-WTC_000033593–000033604

Folder label: “GCMS X 11/19/01 A 12/19 - 12/20/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\DEC1901\27772.D Vial: 28 Acq On : 19 Dec 2001 5:36 pm Operator: 209 GALOS Sample : gc/msunknown 11/19 Inst . - : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Dec 19 18:24 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 14 12:19:30 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 24.98 178 857 / N.D. 34) Anthracene 24.98 178 857 • N.D. 35) Di-n-butylphthalate 27.02 149 2332 • N.D. 36) Fluoranthene 0.00 202 0 N.D. 3 9) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 33.02 228 5220 — N.D. 42) Bis(2-ethylhexyl)phthalate 33.29 149 6147 • N.D. 43) Chrysene 33.02 228 522 0 • N.D. 45) 46) Di-n-Octylphthalate Benzo(b)fluoranthene 35.03 0.00 149 252 176> 0 N.D. N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. 48) Benzo(a)pyrene 37.11 252 5500 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 27772.D GCMS1126.M Mon Dec 31 11:06:45 2001 Page 2

NYC-WTC_000033596

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NYC-WTC_000033596Source: NYC Law Department, mirrored locally

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