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GCMS analysis results, sample AD27826, January 2002

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Gas chromatography-mass spectrometry analysis of environmental sample AD27826 conducted on January 3, 2002, detecting unknown compounds and 2,4-DDD surrogate standard.

NYC-WTC_000033674–000033685

Folder label: “GCMS X 11/19/01 A 12/19 - 12/20/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\DEC1901\27826.D Vial: 32 Acq On : 19 Dec 2001 9:31 pm Operator: 209 GALOS Sample : gc/msunknown 11/19 Inst • : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Dec 19 22:20 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 14 12:19:30 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 24.99 178 1211 / N.D. 34) Anthracene 24.99 178 1211 " N.D. 35) Di-n-butylphthalate 27.01 149 2404 • N.D. 36) Fluoranthene 0.00 202 0 N.D. 3 9) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 33.02 228 5099 Z N.D. 42) Bis(2-ethylhexyl)phthalate 33.29 149 4650 / N.D. 43) Chrysene 33.02 228 5099 N.D. 45) Di-n-Octylphthalate 0.00 149 0 N.D. 46) Benzo(b)fluoranthene 0.00 252 0 N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. 4 8) Benzo(a)pyrene 37.11 252 5729 / N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 27826.D GCMS1126.M Thu Jan 03 11:14:41 2002 Page 2

NYC-WTC_000033677

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NYC-WTC_000033677Source: NYC Law Department, mirrored locally

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