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GCMS analysis results for sample AD26827, Dec 21 2001

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Laboratory report documenting GCMS analysis of sample AD26827 identifying unknown compounds on December 21, 2001.

NYC-WTC_000032160–000032171

Folder label: “GCMS X 11/7/01 A 12/6/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\DEC2701\26827.D Vial: 11 Acq On : 27 Dec 2001 9:53 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Dec 27 22:41 2001 Quant Results File: GCMS1126.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 14 12:19:30 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 24.98 178 1338 N.D. 34) Anthracene 24.98 178 1338 N.D. 35) Di-n-butylphthalate 27.01 149 72176 0.33 ug/1 # 98 36) Fluoranthene 0.00 202 0 N.D. 3 9) Pyrene 29.44 202 266 N.D. 40) Butylbenzylphthalate 31.51 149 544 N.D. 41) Benzo(a)anthracene 33.02 228 5425 N.D. 42) Bis(2-ethylhexyl)phthalate 33.31 149 17799 N.D. 43) Chrysene 33.02 228 5425 N.D. 45) Di-n-Octylphthalate 0.00 149 0 N.D. 46) Benzo(b)fluoranthene 0.00 252 0 N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. 4 8) Benzo(a)pyrene 37.13 252 5221 N.D. 49) Indeno(1,2,3-cd) pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 26827.D GCMS1126.M Fri Dec 28 14:29:16 2001 Page 2

NYC-WTC_000032163

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NYC-WTC_000032163Source: NYC Law Department, mirrored locally

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