NYC-WTC_000035853
Lab notes for sample AD29139 indicate detection of di-n-butylphthalate and one LCS compound outside acceptance range.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Document / 12 pages
GCMS analysis results for sample AD26827, Dec 21 2001
Machine-extracted title · confidence 100%Laboratory report documenting GCMS analysis of sample AD26827 identifying unknown compounds on December 21, 2001.
NYC-WTC_000032160–000032171Folder label: “GCMS X 11/7/01 A 12/6/01”
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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\1\DATA\DEC2701\26827.D Vial: 11 Acq On : 27 Dec 2001 9:53 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Dec 27 22:41 2001 Quant Results File: GCMS1126.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Dec 14 12:19:30 2001 Response via : Initial Calibration DataAcq Meth : GCMS1126
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 11.68 152 1048261 20.00 ug/1 -0.02 10) Naphthalene-d8 15.28 136 4056259 20.00 ug/1 -0.03 17) Acenaphthene-diO 20.56 164 2050252 20.00 ug/1 -0.02 29) Phenanthrene-diO 24.98 188 3103925 20.00 ug/1 -0.01 38) Chrysene-dl2 33.02 240 1937421 20.00 ug/1 -0.01 44) Perylene-dl2 37.12 264 1175695 20.00 ug/1 0.00
System Monitoring Compounds 37) 2,4-DDD 30.06 235 199406 4.44 ug/mL -0.01 Spiked Amount 5.000 Recovery = 88.80%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bi s(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.33 128 1375 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2 -Chioronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 2 2) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.33 165 177 N.D. 25) Diethylphthalate 22.13 149 1583 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 2 7) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration 26827.D GCMS1126.M Fri Dec 28 14:29:12 2001 Page 1
NYC-WTC_000032162
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Lab notes for sample AD29141 indicate detection of bis(2-Ethylhexyl)phthalate and one LCS compound outside acceptance range.
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Laboratory report noting detection of di-n-butylphthalate in sample AD29025 analyzed on December 18, 2001.
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