GCMS analysis results for sample AD27549, Dec 2001

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Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC13 01\27549.D Vial: 8 Acq On 13 Dec 2001 4:45 pm Operator: GALOS Sample : gems unknown 11/15 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 4 Allyldimethylsilane Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

10.29 0.66 ng/uL 216654 1,4-Dichlorobenzene-d4 11.86

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Allyldime ylsilane 100 C5H12Si 003937-30-2 43 2 3-Hexanol 102 C6H140 000623-37-0 42 3 3-Hexanol 102 C6H140 000623-37-0 42 4 3-Hexanol 102 C6H140 000623-37-0 42 Abundance Scan 594 (10.292 min): 27549.D (-) m/z 43.05 1,00.00% 43 59 55 5000- 73 It1 J = 39 85 10.00 10.20 10.40 10.60

m/z-> mm + I 4 t""i' 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 ....ill....... i.......MI m/ z 59.10 63.15% Abundance #1499: Allyldimethylsilane 59

5000- 111 A-IT 10.00 10.20 10.40 10.60 72 85 m/ z 55.1.0 54.58% 100 45 mH X mm TT m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63527: 3-Hexanol 55 59 —A ' ■ I ' • ' ’ I ' 10.00 10.20 10.40 10.60 5000- 73 m/ z 41.10 34.97% 31 I 27 ! TTTTTT ..... 45..... ,tl . 84 I-"•I” "I1 "'I’'"I"' TTTTTTTTTTTTT’T I . I . | . • 1′1′7 < . ! ! I ! I | ! I . I | t > > I | . m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #1762:3-Hexanol ......... S — 1 1 I ' ' ' ■ I ' ' ' ' I ' '

55 59 10.00 10.20 10.40 10.60 m/z 57.10 34.65% 31 5000 27 43 73

TTTTTTTTT TTT TP H— + . ............ ‘IB01BTOOUTI"TTTTTT 102 ‘ ................ _ 1 ‘ I ' 1 1 ' I ' ' TT I ' 1 4 ' m/z--> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 11 10.00 10.20 10.40 10.60

27549.D NP112701.M Fri Dec 14 12:56:48 2001 Page 4

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