GCMS analysis results for sample AD27768, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C : \HPCHEM\ 1 \DATA\DEC1901\27768.D Vial: 11 Acq On 20 Dec 2001 5 :02 am Operator: GALOS Sample gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Hexanone Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

6.49 2.28 ng/uL 759530 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 Z Tentative ID MW MolForm CAS# Qual

1 3-Hexanone 100 C6H120 000589-38-8 91 2 3-He: anone 100 C6H120 000589-38-8 91 3 3-He anone 100 C6H120 000589-38-8 90 4 3-Pentanone, 2-methyl-_______________ 100 C6H120 000565-69-5 47 Abundance Scan 180 (6.489 min): 27768.D (-) m/z 43.10 100.00% 43 57 71 5000 100 6.20 A6.40 6.60 6.80

m/z-> 344 + 51+++ Ppu —1 I' • ’' I ’' " I 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 85 11 m/ z 57.10 94.7)5% Abundance #63357:3-Hexanone 43

5000 29 57

71 i 1 1 6.20 — 6.40 1TT 6.60 6.80 100 m/ z 71.0.5 58.21% 85 I •' "I I'''' I ri + ‘IT r m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63358:3-Hexanone 43 57 l I —4 6.20 d 6.40 6.60 6.80 71 m/z 41.10 28.79% 5000 -

N 100

, 85 I‘‘‘TT r ■ ■' r ■ " i TWTTuTTmmu r rri/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1528: 3-Hexanone 43 • 57 6.20 6.40 6.60 6.80 m/z 100.15 28.12% 29 71 5000 - 100

TT TT+ m ............. . +85 — ITT TTpor " I ■ I' < " I''" I A —........ - m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.80 6.20 6.40 6.60

27768.D NP112701.M Thu Dec 20 11:46:35 2001 Page 1

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