GCMS analysis results for sample AD27767, Jan 2002

NYC 9/11 Public Portal Document

'Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1901\27767.D Vial: 10 Acq On : 20 Dec 2001 4:08 am Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 3-Hexanone Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

6.48 0.83 ng/uL 252218 1,4-Dichlorobenzene-d4 11.87

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 3-He: none 100 C6H120 000589-38-8 90 2 3-He anone 100 C6H120 000589-38-8 78 3 3-H exanone 100 C6H120 000589-38-8 64 4 3- exanone 100 C6H120 000589-38-8 59 'Abundance Scan 179 (6.480 min): 27767.D (-) m/z 43.10 100.00% 43 57

71 5000

39 100 TT .A A . , 84 6.20 6.40 6.60 6.80

miz-> ‘ T 53. 4 1TTTTIT HTTTTTT —mmmm—PPOTT 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 m/ z 57.10 90.27% Abundance #63358:3-Hexanone 43 57

71 t 5000 6.20 6.40 6.60 6.80 100 m/ Z 71 • 05 53.15%

m/z-> Abundance

5000- 20 25 30

29 + 35 40 45 50 55 60 65 70 75 80

43 #1528: 3-Hexanone 57 11 <»1 ■ l ■ ■ ■ ■ I

71 + 85 90 95 100 105

100 " i ■'" r

_A 6.20 m/z 100.15 6.40 6.60 “IPI 6.80 31.47%

85 i " '' i r ■ ‘' i TT i •"' r *1 ’ i ■ ■1 ■ i1 ’1 -1 - - - -J 1" ‘I,I1 * 1 *1 " i" •' r miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63356: 3-Hexanone ■ i ' ' ' ' i ■ ' 29 43 57 6.20 6.40 6.60 6.80 m/ Z 41.10 . 28.21% 5000 71

100

m/z-> " i " '' i ‘ 20 25 —38,4 30 ............... I' । ■ ■ • ■ । ■ ■ ■ ■ । 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 " " i" '' r + 6.20 6.40 6.60 6.80

27767.D NP112701.M Thu Dec 20 11:45:57 2001 Page 1

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