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GCMS analysis results for sample AD27631, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD27631 for unknown compounds and surrogates on January 3, 2002.

NYC-WTC_000033177–000033190

Folder label: “GCMS X 11/16/01 A 12/18 - 12/20/01

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Scanned page image, NYC-WTC_000033185
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC1901\27631.D Vial: 19 Acq On 20 Dec 2001 2:19 pm Operator: GALOS Sample gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Hexanone Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

6.48 1.24 ng/uL 332551 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanone 100 C6H120 000589-38-8 87 2 3-Hexanone 100 C6H120 000589-38-8 87 3 3-H xanone 100 C6H120 000589-38-8 72 4 3- exanone 100 C6H120 000589-38-8 59 Abundance Scan 178 (6.477 min): 27631.D (-) m/ z 43.10 100.00% 43 57 71 5000 100 TIT --- 6.20 6.40 6.60 6.80 ' I " '111 tt 53.-344 . .......... . 85 TTTTTT I " * ‘ I p m/ z 57 • 10 90.69% m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63358: 3-Hexanone 43

U 57

71 ) . , . pT-T-r-r-pr-r-r-r TIIrrrm 5000- 6.20 6.40 6.60 6.80 100 m/z 71.05 55.14% 85 111. ,| rr, , । ■,,, । +T p-rrrp- TT‘ miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 35 90 95 100 105 Abundance #1528: 3-Hexanone 43 57 i / I 6.20 6.40 6.60 6.80 29 71 m/z 100.15 30.71% 5000 - 100 । ’T’II 85 11'111 TTTTTTT’TTTTT I •' " I r m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63356: 3-Hexanone -r-T-pr-r-r-r-r-f-r ■ ' I ' ' 29 43 57 6.20 6.40 6.60 6.80 m/ Z 41.05 26.29%

NW 5000 - 71

100

m/z-> " i" " r 38 r " ■ i'' " i .. . i' ■ " r " ' i tmmm " '' i"'' r 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.20 6.40 6.60 6.80

27631.D NP112701.M Fri Dec 21 09:19:50 2001 Page 1

NYC-WTC_000033185

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NYC-WTC_000033185Source: NYC Law Department, mirrored locally

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