GCMS analysis results for sample AD27956, Jan 2002

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Data File : C: \HPCHEM\ 1 \DATA\DEC190127956.D Vial: 12 Acq On : 21 Dec 2001 2 :12 am Operator: GALOS Sample : gems unknown 11/20 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Hexanone Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

6.45 0.64 ng/uL 208012 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 / Tentative ID MW MolForm CAS# Qual

1 3-Hexanone 100 C6H120 000589-38-8 91 2 3-He:xanone 100 C6H120 000589-38-8 90 3 3-HaAanone 100 C6H120 000589-38-8 90 4 3-He xanone 100 C6H120 _______ 000589-38-8 78 Abundance Scan 176 (6.455 min): 27956.D (-) m/z 43.10 . 100.00% 43 57

71 5000 100 ’ ’’1111111 6.20 6.40 6.60 6.80 -------314 53. , 85 1TTNITTTTH "I.............. 1............ . . . I.. ................ m/z 57.10 89.93% miz- 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1528: 3-Hexanone 43 57

29 71 — । , — , TIT TTr12 5000 6.20 6.40 6.60 6.80 100 m/z 71.05 50.90% "T""|lr. 111 ■' 111111! I 'I"......... I' ................ . .......... miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63358. 3-Hexanone 43 57

71 Ai ■■ ■ ■ i

6.20 LA 6.40 6.60 6.80 5000 m/z 100.15 28.32% 100

i 85 111111 | | |■■■■| 'I' ■ ■ 11 " • 7-i I t. । ■ ■. ■ । ■ ■ ■ ■ |. u ■ ■ ■ ■ । ■ ■ ■ I" " I m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63357: 3-Hexanone I 43 6.20 6.40 6.60 6.80 57 29 m/z 41.10 23.07%

miz-> 5000

mp mm ..... .......... +ttt I" ' ’ f 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 71

85 100

6.20 MW 6.40 6.60 6.80

27956.D NP112701.M Fri Dec 21 10:00:31 2001 Page 1

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