GCMS analysis results for sample AD27765, Jan 2002

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Laboratory report documenting GCMS analysis of sample AD27765 for unknown compounds and surrogates on January 3, 2002.

NYC-WTC_000033311–000033342

Folder label: “GCMS X 11/16/01 A 12/18 - 12/20/01”

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NYC 9/11 Public Portal Document

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Data File : C:\HPCHEM\1\DATA\DEC1901\27765.D Vial: 8 Acq On : 20 Dec 2001 2:18 am Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 2 Oxepane, 2,2,4-trimethyl- Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

5.10 1.38 ng/uL 309447 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Oxepane, 2,2,4-trimethyl- 100 C6H120 023120-44-7 36 2 1-Hexene 84 C6H12 000592-41-6 33 3 1-Hexene 84 C6H12 000592-41-6 33 4 Hexylene Glycol__________________ 118 C6H14O2 000107-41-5 10 'Abundance Scan 28 (5.098 min): 27765.D (-) m/z 41 ,10 100.00% 41 56

5000-

71 I''1 ‘ I i" ' • ।■ i ■ i ■ ■ " i

m/z-> TH ++ 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110115 | 4 1np—n—np—mu*anup—B—pBnpuu 77 82 93 109 TNTHT 4.90 5.00 5.10 5.20 5.30 5.40 5.50 m/z 56.10 77.44% Abundance #1525: Oxepane, 2,2,4-trimethyl- 43 59

5000 i'111 r 111111111 ■ ‘111 TT 4.90 5.00 5.10 5.20 5.30 5.40 5.50 m/z 59 70.75% 31 100 85 m/z-> I" " I Tim Hm ।" " f"1TTTTTTTT I' ’' • I TITT TTTTTT’TTT 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110 115 i

Abundance #62755: 1-Hexene 41 56 27 TA 4.90 5.00 5.10 5.20 5.30 5.40 5.50 5000- m/z, 42.10 59.53% 84 69 i” ''i1 i' ''Vj 51 / ■ r । i i i i । ii i i । ii i i। i i ■ i । > i ii । i I । i i i ■J TTTTTTTTTTT TTTTT’TT T ’TTTTTTTTT m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 115 Abundance #62753:1-Hexene F’'’11 TTT 41 56 4 90 5.00 5.10 5.20 5.30 5.40 5.50 m/z. 43.10 52.15% 5000- 27 84 69

miz-> ...+...... 4 ‘I I’’’•I 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110115 IH "I'1 ’' I p I l i | t i M | I I I I | I 11«| I । । • I I | TUIUmman 11' " I' " ' I 4.90 5.00 5.10 5.20 5.30 5.40 5.50

27765.D NP112701.M Thu Dec 20 11:44:34 2001 Page 2

NYC-WTC_000033333

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GCMS analysis results for sample AD27679, Jan 2002 · Box DEP Box 21

NYC-WTC_000033263

Laboratory report documenting GCMS analysis of sample AD27679 for unknown compounds and surrogates on January 3, 2002.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998