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GCMS analysis results for sample AD27764, Jan 2002

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD27764 for unknown compounds and surrogates on January 3, 2002.

NYC-WTC_000033285–000033310

Folder label: “GCMS X 11/16/01 A 12/18 - 12/20/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\l\DATA\DEC1901\27764.D Vial : 7 Acq On : 19 Dec 2001 12:38 pm Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : .TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 4.995 3 17 23 rBV 31215 222646 3.42% 0.538% 2 5.124 28 31 35 rW 366932 623955 9.58% 1.507% 3 5.188 35 38 54 rVB 532696 972137 14.92% 2.348% 4 5.610 81 84 88 rW 55208 105312 1.62% 0.254% 5 5.674 88 91 99 rVB 79319 151901 2.33% 0.367%

6 6.114 135 139 153 rVB 343983 686594 10.54% 1.658% 7 6.462 172 177 184 rBV 128347 250445 3.84% . 0.605% 8 6.563 184 188 198 rVB 155715 310468 4.77% 0.750% 9 6.692 198 202 210 rBV 157852 314288 4.82% 0.759% 10 6.811 210 215 219 rBV2 112625 246034 3.78% 0.594%

11 6.912 223 226 232 rVB2 33292 66896 1.03% 0.162% 12 7.022 232 238 243 rVB 37513 79112 1.21% 0.191% 13 7.168 244 254 259 rBV 1364416 3192240 49.01% 7.710% 14 7.765 314 319 323 rBV 36166 66326 1.02% 0.160% 15 7.829 323 326 33 9 rVB 207095 416255 6.39% 1.005%

16 9.314 481 488 500 rBV 135077 277351 4.26% 0.670% 17 10.286 589 594 604 rBV 743518 1432645 21.99% 3.460% 18 10.488 611 616 626 rBV 520554 1003553 15.41% 2.424% 19 10.818 647 652 660 rVB 91859 171093 2.63% 0.413% 20 11.854 759 765 774 rVB 2388516 5064033 77.74% 12.231%

21 15.458 1151 1158 1173 rBV 2997264 6513753 100.00% 15.733% 22 20.731 1725 1733 1742 rBV 2904084 6189423 95.02% 14.949% 23 25.142 2206 2214 2225 rBV2 2627870 5564845 85.43% 13.441% 24 33.138 3079 3086 3102 rBV2 1786170 4163130 63.91% 10.055% 25 37.219 3523 3531 3547 rBV2 1214072 3318459 50.95% 8.015%

Sum of corrected areas: 41402894

NYC-WTC_000033291

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NYC-WTC_000033291Source: NYC Law Department, mirrored locally

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