GCMS analysis results for sample AD27627, Jan 2002

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Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1901\27627.D Vial: 17 Acq On : 20 Dec 2001 12:30 pm Operator: GALOS Sample : gems unknown 11/16 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title 208 625/TCLP calibration table Library C: \DATABASE\NBS75K. L ********************************************************************* Peak Number 1 3-Hexanone Concentration Rank 4

R.T. ■EstConc Area Relative to ISTD R.T.

6.48 1.04 ng/uL 330695 1,4-Dichlorobenzene-d4 11.87

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanone 100 C6H120 000589-38-8 91 2 3-Hexanone 100 C6H120 000589-38-8 86 3 3 - Hexanone 100 C6H120 000589-38-8 83 4 Pentane, 2,3,4-trimethyl -________ 114 C8H18 000565-75-3 53 Abundance Scan 179 (6.483 min): 27627.D (-) m/z 43.10 100.00% 43 57 71 5000 100 — TT - 39 6.20 6.40 6.60 6.80

miz-> - —4 53, .............H 111" " i"111' +1 85 TIr V'" I 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 m/z 57.10 92.41% Abundance #63358:3-Hexanone 43 57 _ r 71 5000 6.20 6.40 6.60 6.80 100 m/z 71.05 58.22% I»1 1 11 • 1 1 1 I '1'' I " ' ' I 'I....... "I' . ...... p m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1528: 3-Hexanone 43 57 6.20 6.40 6.60 6.80 29 71 5000 m/ z 100.15 30.01% 100 85 | PI I> I r q. > I I I I ” •' I TTTTTTTTTTTTTTTTTTTTTTT ’TTT T1 m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63357:3-Hexanone - 43 6.20 6.40 >.60 6.80 57 m/ z 41.10 28.34% 29 5000-

mpm । । ■ ■1' । ■' ■ ■ i'1 111"11" " I' T’ITTT 85 T—UT0’’T 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 100 71

r 6.20 TPfT 6.40 M 6.60 6.80

27627.D NP112701.M Fri Dec 21 09:18:09 2001 Page 1

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