GCMS results log, sample AD26985, Dec 11 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0601\26986.D Vial: 32 Acq On 7 Dec 2001 3:19 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 5 2-Propanone, 1-methoxy- Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

7.18 1.01 ng/uL 401367 1,4-Dichlorobenzene-d4 11.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Propanone, -methoxy- 88 C4H802 005878-19-3 9 2 2-Butanol, -methyl- 88 C5H120 000598-75-4 9 3 Propane, /-ethoxy- 88 C5H120 000625-54-7 9 4 1,4-But ediamine 88 C4H12N2 000110-60-1 7 Abundance Scan 255 (7.177 min): 26986.D (-) m/z 45.10 100.00% 45

A 5000 61 73 4:

m/z-> 5 10 15 I" ” I 20 25 30 4 4-56— 35 40 45 50 55 60 65 70 70 + 75 80 88 TTTHT 85 90 95 6.80 m/ z 7.00 43.0.0 7.20 7.40 89.60% 7.60

Abundance #62920: 2-Propanone, 1-methoxy- 45

5000 TTTmm 29 58 6.80 7.00 7.20 7.40 7.60 15 42 m/z 61.00 31.98% . TTi T TTT 26 38 1 TTTT- J .-n-rpn-rrp-r- T‘UE‘FETTTTTT“T"TTT‘‘I‘T 88 I" " I m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #62961: 2-Butanol. 3-methyl- 45

6.80 7.00 7.20 7.40 7.60 5000- m/z 73.0,5 29.11%

, 55 73 27 31 1 59 69 87 TTTTTTWTTTIWWTWNTNWTTT TITTTTINIT TITrr I " '' I' ’ ’ ’ I''' • I'''' I" m/z-> Abundance 5 m 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 #62956: Propane, 2-ethoxy- 45 A.... R 6.80 7.00 7.20 7.40 7.60 m/z 44.00 20.76% 5000 73 27 15 31 3942 59 88 TT - TITTTTTT I I | ! I I I | I I I I | I I TTCTUu m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 6.80 7.00 7.20 7.40 7.60

26986.D NP112701.M Tue Dec 11 14:51:27 2001 Page 5

NYC-WTC_000032413