GCMS analysis results, sample AD28432, November 2001

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Library Search Compound Report Data File C:\HPCHEM\1\DATA\DEC0501\28432.D Vial: 4 Acq On 5 Dec 2001 3:34 pm Operator: 209 GALOS Sample re extract Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Propanol, 1-(2-methoxy-1-met Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 11.47 0.42 ug/1 96716 1,4-Dichlorobenzene-d4 11.71 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 2-Propanol, 1-(2-methoxy-1-methylet 148 C7H16O3 020324-32-7 78 2 2-Butanol, 3,3' -oxybis- 162 C8H18O3 054305-61-2 39 3 Silane, ethyldimethyl- 88 C4H12Si 000758-21-4 36 4 1-Propanol, 2- (2-hydro3cypropoxy) - 134 C6H14O3 000106-62-7 36 Abundance Scan 700 (11.473 min): 28432.D (-) m/z 59.05 100.00% 59

5000 45 103 73 ■ 1 i ■ ■ 11.20 11.40 11.60 11.80 391, 85

N < i • • ■ ■ i ‘ ■ — —TTH 1 ' I 1 ' i ■ ' ' ■ i ' - m/ Z 45.00 46.50% mlz—> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #9238: 2-Propanol, 1-(2-methoxy-1-methylethoxy)- 59

5000 •IT "I I ' ' i » I • I I < I • I l’ < 45 103 11.20 11.40 11.60 11.80 73 31 m/z 103.05 37.73% — . . . . I TTH A T i TP .......... -IPPP i 1 ■ ■ ■ i ■ ' ■ 130 ' i 11 ' 1 i ■ miz-> 20 30 40 50 60 70 80 90 100 11 0 120 130 140 Abundance #12859:2-Butanol, 3,3‘-oxybis- 59 I-P —T —TY —MAAr r 1 11.20 11.40 11.60 11.80 5000 31 m/z 73.00 27.44% 45 103

m/z-> Abundance 20 —l TIIr —+ 30 40 50 60

59 70 80 90 . 100 110 #844: Silane, ethyldimethyl- 120 ... 134 130 1 40 TTPITT

m/z NN. 11.20 11.40 11.60 11.80

V 41.00 26.67% 5000- 45 73 87 - AMM “YAM ' l 1111I 1 ' 1 1. ' । 1 I 1 m/z—> 20 30 40 50 60 70 80 90 100 110 120 130 140 11.20 11.40 11.60 11.80

28432.D GCMS1126.M Thu Dec 06 11:45:43 2001 Page 2

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