GCMS calibration table for TCLP analysis, Dec 5 2001

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Calibration data sheet listing standard compounds and response factors used for GCMS analysis on December 5, 2001.

NYC-WTC_000032142–000032159

Folder label: “GCMS X 11/7/01 A 12/6/01”

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Data File C:\HPCHEM\l\DATA\DEC0501\26712.D Vial: 3 Acq On 5 Dec 2001 10:35 am Operator: GALOS Sample gc/ms unknown 11/7 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 2-Butanol, 3-methyl-, (S) - Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

7.16 6.54 ng/uL 2288020 1,4-Dichlorobenzene-d4 11.86

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Butanol, /3-methyl - , (S) - 88 C5H120 001517-66-4 42 2 2,3-Butanediol 90 C4H10O2 000513-85-9 33 3 N-Ethyl formamide 73 C3H7NO 000627-45-2 9 4 2-Butangl, 3-methyl- 88 C5H120 000598-75-4 9 Abundance Scan 252 (7.156 min): 26712.D (-) m/z 45.05 100.00% 45

5000 - 61 73

6.80 7.00 7.20 7.40 7.60 T" "I i"" 35 1 i" "i — tm 88 !।i ।।... ।.... ।.... 11TTTTT i-i 1111111 207 TTTT m/z 43.00 59.92% m/z—> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #852: 2-Butanol, 3-methyl-, (S)- 45

5000 T'1 1 1r"IT 1 6.80 7.00 7.20 7.40 7.60

73 m/z 73.05 35.72% 27 55 m/z-> TT H 1 87 I" "I" "I"111 !।।।! ‘T‘T‘"Ti 111111111111 rqrriT| 11111 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 200210 'Abundance #917: 2,3-Butanediol 45 - _ 4 6.80 7.00 7.20 7.40 7.60 5000 m/z 61.10 35.24% 29 19 57 75 90 TT)T ।* ■«■ । ■ * > • । । ‘IUTTTTTTTTTTi TT m/z-> Abundance 10 20 30 40 50 60 70 80 90 100110120130140150160170180190 200210 #292: N-Ethylformamide — 4 ,, 30 6.80 7.00 7.20 7.40 7.60 73 m/z 44.05 12.16% 5000 44 58

m/z-> xl M I ■ ■" I > l ■ • l" ■ ■ l ■ ■" I'" ■ l •" ' l >" • i • ■ ‘ ’ 111" 111111 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 " 11111111111"111111 T’" 1 ■ i ■ TCT <■. । । । > । । । । < । । । । । 6.80 7.00 7.20 7.40 7.60

26712.D NP112701.M Fri Dec 07 13:15:15 2001 Page 5

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