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GCMS analysis results for sample AD26679, Dec 10 2001

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Laboratory report documenting GCMS analysis of sample AD26679 identifying unknown compounds on December 10, 2001.

NYC-WTC_000032028–000032057

Folder label: “GCMS X 11/7/01 A 12/6/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\DEC0401\26679.D Vial: 5 Acq On 4 Dec 2001 2:27 pm Operator: GALOS Sample gc/ms unknown Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 18 10-Methylnonadecane Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

33.73 1.10 ng/uL 233623 Chrysene-dl2 33.17

Hit# of 5 Tentative ID MW MolForm CAS# Qual & 1 10-Methylnonadecane 282 C20H42 000000-00-0 2 Dotriacontane 451 C32H66 000544-85-4 3 Nonadecane 268 C19H40 000629-92-5 90 4 Tetratetracontane 619 C44H90 007098-22-8 90 Abundance Scan 3151 (33.735 min): 26679.D (-) m/z 57. 10 100.00% 57

5000 85 A Z s.... I TI ‘l 207 33.40 33.60 33.80 34.00 m/ Z 4 3.10 69.07% miz-> 50 100 150 200 250 300 350 400 450 Abundance #39858: 10-Methylnonadecane 57

5000 85 A— 33.40 33.60 33.80 34.00 154 m/z 71.05 65.09% I 1113 1 m/z-> 50 100 150 200 250 300 350 400 450 Abundance #74491; Dotriacontane 57 — —......................

33.40 33.60 33.80 34.00 5000 85 m/z 85.05 41.39%

113 I I 141 » 1 196 281 422 450 • ' 1 I m/z-> 50 100 150 200 250 300 350 400 450 Abundance #37469: Nonadecane > । i ■ ■ ■ । > ■ > ■ । I 7 33.40 33.60 33.80 34.00 m/z 55.10 28.98% 85 5000

m/z-> I 50 1 ‘13100 150 183 200 250 268 300 350 400 450 -.. L4..... 33.40 33.60 33.80 34.00

26679.D NP112701.M Fri Dec 07 13:10:35 2001 Page 18

NYC-WTC_000032053

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NYC-WTC_000032053Source: NYC Law Department, mirrored locally

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