GCMS analysis sample AD26537, non-target compounds, Dec 2001

NYC 9/11 Public Portal Document Library Search Compound Report

Data File C: \HPCHEM\ 1 \DATA\DEC0 701\26537.D vial: 4 Acq On 7 Dec 2001 8:51 pm Operator: GALOS Sample gc/ms unknown 11/6 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 3-Hexanone Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 6.44 0.73 ng/uL 195450 1,4-Dichlorobenzene-d4 11.88

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Hexanone 100 C6H120 000589-38-8 86 2 3-Hexanone 100 C6H120 000589-38-8 83 3 3-Hexanone 100 C6H120 000589-38-8 59 4 3-Pentanone, 2-methyl - 100 C6H120 _______ 000565-69-5 47 Abundant Scan 174 (6.438 min): 26537.D (-) m/z 43.10 100.00% 43 57

5000

i■ ‘ “ i■ mH H53,, 36 I , , 85 H tmmmmmm 71 100

' i ■ ■" i J_N 6.00 8.20 6.40 6.60 ' 6.80 m/z 57.1,0 97.62% miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #83358: 3-Hexanone 43 57

71 5000 ■ • i ■ ■ ■ • i ■ ■ ‘ ■ i ■ ■ ■ ■ i ‘ 6.00 S.20 6.40 6.60 6.80 100 m/z 71.05 52.26% | J 4 ||| I I Ipatr +mp *m ._______ —apa 85 ‘‘' I ‘‘ • I m/z—> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1 528: 3-Hexanone — i — 43 57 *P—1—----FITr 6.00 6.20 6.40 6.60 6.80 29 71 m/z 100.15 33.09% 5000

k 100 i, —h}——TEnap_p85 1 ■ ■ ‘i■■ ■ • i miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance 29 #63356:3-Hexanone 43 57 WM *I»» 1 ’I1' 1 »I»»» 6.00 6.20 6.40 6.60 6.80 m/z 41.00 23.83% 5000 71

m/z-> —38, -rrrp-rrrp- TIUIU-110, tmmm 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 100 MAM 6.00 6.20 6.40 ' 6.60 6.80

26537.D NP112701.M Thu Dec 13 11:27:19 2001 Page 6

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