GCMS calibration data for TCLP analysis dated December 7, 2001

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Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC0 7 01\LB.D Vial: 2 Acq On 7 Dec 2001 7:01 pm Operator: GALOS Sample gc/ms unknown 11/6 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 3-Hexanone Concentration Rank 12

R.T. EstConc Area Relative to ISTD R.T.

6.44 0.76 ng/uL 234102 1,4-Dichlorobenzene-d4 11.88

Hit# of 5 Tentative ID MW Mol Form CAS# Qual

1 3-Hexanone 100 C6H120 000589-38-8 91 2 3-Hexanone 100 C6H120 000589-38-8 91 3 3 -Hexanone 100 C6H120 000589-38-8 91 4 3-Hexanone 100 C6H120 000589-38-8 53 Abundance Scan 175 (6.444 min): LB.D (-) 100.00% 43 57

71 5000 100 I ‘ 1 1 * I ‘ ' I ' ‘ ’ 1 I 4 1 1 ‘ I 1 ‘ ‘ 39 mmmmm +5++ 6.00 6.20 6.40 6.60 6.80 85 Hpam] 11.।| |a... ।.... "• ‘I' '"I m/z 57.1.0 85.31% miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63358:3-Hexanone 43 57

71 5000 6.00 6.20 6.40 6.60 6.80 100 m/z 71.05 52.51% , 85 m mmm11 m Ipmp Hmm " "i ■ ” ■ i miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1528: 3-Hexanone 43 57

29 71 6.00 6.20 6.40 6.60 16.80— 5000 m/z 100.05 27.85%

mfe-> Abundance

5000 ] 1 ,85 100

I >. 1111111 U 111111111..! H I. |.. 1111 > > 11111111 n 11 n 111111. |. 11. |.... j... 11 > > > 11111 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105

29 #63357:3-Hexanone 43 57

71 "' I “ " I

M 1 A6.20..6.40 6.60 6.80 6.00 rn/

100 TIT . ..........। • i ■ ■ ■ ■ i ■' ■ ■ i • .85 m/z—> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.00 6.20 6.40 6.60 6.80

LB.D NP112701.M Thu Dec 13 11:28:32 2001 Page 6

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