GCMS Analysis Report for Sample AD26337, Dec 2001

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Data File C:\HPCHEM\1\DATA\NOV3 001\26337.D Vial: 25 Acq On 1 Dec 2001 10:01 am Operator: GALOS Sample gc/ms unknown 11/3 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 5 Hexane, 1-propoxy- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

10.32 0.79 ng/uL 210827 1,4-Dichlorobenzene-d4 11.89

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexane, 1-pro OxY- 144 C9H20O 053685-78-2 25 2 Oxirane, 2-ms' hyl-3-propyl-, cis- 100 C6H120 006124-90-9 12 3 Pentanal, 2-methyl- 100 C6H120 000123-15-9 9 4 Hexane, 2 -methyl - 100 C7H16 000591-76-4 9 'Abundance : Z Scan 597 (10.320 min): 26337.D (-) m/z 43.10 100.00% 4

5000 - 55 59

39 73 85 XA 10.00 10.20 10.40 10.60 mmmmmmP + 89 TT — 100 r ''' r ' ।" " । —HH m/z 59.1.0 37.62% miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #8516: Hexane, 1-propoxy- 43

5000 - I- 10.C 10.20 10.40 10.60 56 85 m/z 57.1,0 35.94% 73 Hmm 9 I 61 39

miz-> 20 ‘h‘ i ■■ ■ • i 4 pu 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 TT‘ ‘‘1‘‘‘‘11‘ttT’rr’

'Abundance #1531: Oxirane, 2-methyl-3-propyl-. cis- 43 - TAT 57 10.00 10.20 10.40 10.60 5000 71 85 m/ Z 55.10 35.25% I

I 111111TTITTT • । | < ! H ] l l . . | > ! ! . | 100 . | . . ■ 1 ■ ■■ । ■ ■' ■ । ■ ■ ■ ■ । ■ ■ "i ■ ■" । I'' ■ ■ r ■ ■ ■ i m/z-> Abundance 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 #63343: Pentanal, 2-methyl- yA — TIITT r । 43 10.00 10.20 10.40 10.60 58 m/ z 41.10 31.48% 5000

27 71

miz-> 38 4 | • ' ' ' j ' । i I | I I H j • i • i | H +H100 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 I ' i ■ ■'' i1" ' r " ' i'' " i TT '' i " " I' " ' i'''' i'''' i - | A4A r A APr I J I Fil -A t44—T 10.00 10.20 10.40 10.60

26337.D NP112701.M Fri Dec 21 14:28:54 2001 Page 5

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