GCMS calibration table, Dec 2001

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File C: \HPCHEM\1\DATA\NOV3 0 01\LBA. D 2(7 OS Vial: 15 Acq On 1 Dec 2001 12:56 am A 12<— L . Operator: GALOS Sample Mise 1 11/5 MS Integration Params: RTEINT.P -59 14/373 7 Inst Multiplr: : GC/MS Ins 1.00 Quant Time: Dec 3 15:25 2001 26%) D.7 ‘ "Quant Results File: NP112701.RES Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Last Update : Wed Nov 28 15:33:44 2001 Response via : Initial Calibration DataAcq Meth : NP112701

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.89 152 942284 20.00 ng/uL -0.04 19) Naphthalene-d8 15.51 136 3626005 20.00 ng/uL -0.04 31) Acenaphthene-diO 20.78 164 1635923 20.00 ng/uL -0.04 49) Phenanthrene-diO 25.18 188 2301552 20.00 ng/uL -0.06 59) Chrysene-dl2 33.19 240 1406476 20.00 ng/uL -0.06 68) Perylene-dl2 37.28 264 990432 20.00 ng/uL -0.06

System Monitoring Compounds 4) 2-Fluorophenol 0.00 112 0 0.00 ng/uL Spiked Amount 75.000 Range 18 42 Recovery = 0.00%# 5) Phenol-d5 0.00 99 0 0.00 ng/uL Spiked Amount 75.000 Range 19 32 Recovery = 0.00%# 6) 2-Chlorophenol-d4 11.88 132 292 0.00 ng/uL 0.46 Spiked Amount 75.000 Range 34 84 Recovery = 0.00%# 7) 1,2-Dichlorobenzene-d4 12.21 152 851 0.02 ng/uL -0.25 Spiked Amount 50.000 Range 26 73 Recovery = 0.04%# 20) Nitrobenzene-d5 0.00 82 0 0.00 ng/uL Spiked Amount 50.000 Range 55 98 Recovery = 0.00%# 32) 2-Fluorob ipheny1 18.93 172 1356 0.01 ng/uL 0.10 Spiked Amount 50.000 Range 42 78 Recovery = 0.02%# 33) 2,4,6-Tribromophenol 0.00 330 0 0.00 ng/uL Spiked Amount 75.000 Range 45 96 Recovery = 0.00%# 62) Terphenyl-dl4 0.00 244 0 0.00 ng/uL Spiked Amount 50.000 Range 58 98 Recovery = 0.00%# Target Compounds Qvalue 2) Pyridine 0.00 79 0 N.D. 3) N-nitrosodimethylamine 0.00 74 0 N.D. 8) Phenol 0.00 94 0 N.D. 9) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 10) 2-Chlorophenol 0.00 128 0 N.D. 11) 1,3-Dichlorobenzene 0.00 146 0 N.D. 12) 1,4-Dichlorobenzene 0.00 146 0 N.D. 13) 1,2-Dichlorobenzene 0.00 146 0 N.D. 14) 2-Methylphenol 0.00 108 0 N.D. 15) 2,2' -oxybis(1-Chloropropan 0.00 45 0 N.D. 16) 3&4-Methylphenol 0.00 108 0 N.D. 17) N-Nitrosodi-n-propylamine 0.00 70 0 N.D. 18) Hexachloroethane 0.00 117 0 N.D. 21) Nitrobenzene 0.00 77 0 N.D. 22) Isophorone 0.00 82 0 N.D.

(#) = qualifier out of range (m) = manual integration LBA.D NP112701.M Tue Dec 04 08:19:22 2001 Page 1

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