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GCMS analysis results for sample AD26317, Dec 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD26317 with unidentified compounds detected.

NYC-WTC_000031274–000031283

Folder label: “GCMS X 11/3/01 A 12/1/01

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Scanned page image, NYC-WTC_000031281
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV3001\26317.D Vial: 16 Acq On : 1 Dec 2001 1:51 am Operator: GALOS Sample : gc/ms unknown 11/3 Inst : GC/MS Ins Mise 2 Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Hexane, 1-propoxy­ Concent rat ion Rank 4 R.T. EstConc Area Relative to ISTD R.T. 10.33 0.41 ng/uL 188927 1,4-Dichlorobenzene-d4 11.90 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Hexane, 1-propoxy- 144 C9H20O 053685-78-2 12 2 2,2-Dimethy 1,3-propanediamine 102 C5H14N2 007328-91-8 10 3 Butane / 58 C4H10 000106-97-8 9 4 3-Hexanol/2-methyl- 116 C7H160 000617-29-8 9 Abundance 7 Scan 598 (10.328 min): 26317.D (-) m/z 43.05 100.00% 43

5000- 59 55 85 "—I T 39 73 10.00 10.20 10.40 10.60

miz-> 5 m + lm + 1 mm -9— m/z 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 59.10 41.46% Abundance #8516: Hexane, 1-propoxy- 43

5000 10.00 10.20 10.40 10.60 56 73 K m/z 57.10 35.60%

miz-> L510 ______ lLlle 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #1751:2,2-Dimethyl-1,3-propanediamine 30 70 —-A——. -A— 4AA 10.00 10.20 10.40 10.60 5000 56 m/z 55.10 32.01% 85 73 27 42 1 I 1111 p 1111111111ri11.1>.In.I।।।1111.।।n 1.1111.j..i. ।|।।. m/z—> Abundance 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95

43 #62336: Butane -4 10.00 10.20 10.40 10.60 m/z 41.10 30.24%

L 5000 29

39 58 15 26 1AnA 444 a - mHHlll miz—> 5i 10 15 20253035404550556065 70 75 80859095 10.00 10.20 10.40 10.60

26317.D NP112701.M Tue Dec 04 10:12:23 2001 Page 3

NYC-WTC_000031281

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NYC-WTC_000031281Source: NYC Law Department, mirrored locally

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