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GCMS analysis results for sample AD26204, Dec 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GCMS analysis of sample AD26204 with unidentified compounds detected.

NYC-WTC_000031129–000031158

Folder label: “GCMS X 11/2/01 A 12/1/01

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NYC 9/11 Public Portal Document

• Library Search Compound Report

Data File : G:\HPCHEM\1\DATA\DEC0401\26205.D Vial: 68 Acq On : 4 Dec 2001 10:25 am Operator: 209 GALOS Sample : 11/2 gc/ms Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP112601.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 1,4-Dichlorobenzene-d4 Concentration Rank 18

R.T. EstConc Area Relative to ISTD R.T. --------------------------------------------------------------------- 11.57 0.61 ug/1 171064 1,4-Dichlorobenzene-d4 11.70

Hit# of 5 Te- ative ID MW MolForm CAS# Qual ---------------- --------------------------------------------------- 1 1,4-Dichloro nzene-d4 150 C6C12D4 003855-82-1 58 2 Benzene-1,2, ,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 25 3 Acenaphthyl ne 152 C12H8 000208-96-8 10 4 Benzaldeh e, 2-h droxy-3-metho - 152 C8H803 000148-53-8 9 thundance Scan 710 (11.565 min): 26205.D (-) m z 149. 90 100. 00% 1

5000 115

52 78 38 87 11.20 11.40 11.60 11.80 99 m z 151.90 61.34% _> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 thundance #9593:1,4-Dichlorobenzene-d4 1

J000 115 52 78 11.20 11.40 11.60 11.80 m/z 115.00 38.94% 87

rilz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 bundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 1

115 11.20 11.40 11.60 11.80 5000 52 78 m/z 78.05 18.6l

35 87

rift-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 ndance #67013: Acenaphthylene 12 11.20 11.40 11.60 11.80 m/z 52.00 17.34%

5000

76 63 I 126 110 120 130 1

26205.D NP112601.M Tue Dec 04 15:58:33 2001 Page 3

NYC-WTC 000031140

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NYC-WTC_000031140Source: NYC Law Department, mirrored locally

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