Calibration data for GC/MS analysis using Method 508 and TCLP procedures dated November 30, 2001.
NYC-WTC_000030923–000030932Folder label: “GCMS SCAN X 11/2/01 AN 11/30/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
f Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\NOV3 001\LBD.D vial: 51 Acq On : 30 Nov 2001 3:40 pm 050 — Ro Operator: 209 GALOS Sample Mise : 16 11/2 967ms MS Integration Params: RTEINT.P 007-33 Inst : GC/MS 209 Multiplr: 1.00 \63 Quant Results File: NP112601.RES Quant Time: Nov 30 16:29 2001 Quant Method : C:\HPCHEM\1\METHODS\NP112601.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Nov 27 09:03:50 2001 Response via : Initial Calibration DataAcq Meth : NP112601
Internal Standards R.T. Qlon Response - Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.70 152 1044772 20.00 ug/1 0.00 19) Naphthalene-d8 15.31 136 4036500 20.00 ug/1 0.00 31) Acenaphthene-diO 20.58 164 1901292 20.00 ug/1 0.00 4 9) Phenanthrene-dl0 25.00 188 2615781 20.00 ug/1 0.01 59) Chrysene-dl2 33.03 240 1424704 20.00 ug/1 0.00 68) Perylene-dl2 37.12 264 894682 20.00 ug/1 0.00 System Monitoring Compounds 4) 2-Fluorophenol 0.00 112 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 5) Phenol-d5 0.00 99 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 6) 2-Chlorophenol-d4 11.70 132 674 0.01 ug/1 0.50 Spiked Amount 75.000 Recovery = 0.01% 7) 1,2-Dichlorobenzene-d4 12.23 152 11616 0.26 ug/1 0.01 Spiked Amount 50.000 Recovery = 0.52% 20) Nitrobenzene-d5 0.00 82 0 0.00 ug/1 Spiked Amount 50.000 Recovery = 0.00% 32) 2-Fluorobiphenyl 18.73 172 4251 0.04 ug/1 0.15 Spiked Amount 50.000 Recovery = 0.08% 33) 2,4,6-Tribromophenol 0.00 330 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 62) Terphenyl-dl4 0.00 244 0 0.00 ug/1 Spiked Amount 50.000 Recovery = 0.00% Target Compounds Qvalue 2) Pyridine 5.37 79 381 N.D. 3) N-nitroso-dimethyl amine 5.50 74 107 N.D. 8) Phenol 10.93 94 123 N.D. 9) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 10) 2-Chlorophenol 0.00 128 0 N.D. 11) 1,3-Dichlorobenzene 0.00 146 0 N.D. 12) 1,4-Dichlorobenzene 0.00 146 0 N.D. 13) 1,2-Dichlorobenzene 0.00 146 0 N.D. 14) 2-Methylphenol 0.00 108 0 N.D. 15) 2,2' -oxybis(1-Chloropropan 0.00 45 0 N.D. 16) 3&4-Methylphenol 0.00 108 0 N.D. 17) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 18) Hexachloroethane 0.00 117 0 N.D. 21) Nitrobenzene 12.99 77 191 N.D. 22) Isophorone 0.00 82 0 N.D. (#) = qualifier out of range (m) = manual integration LBD.D NP112601.M Mon Dec 03 09:11:55 2001 Page 1
NYC-WTC_000030923
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NYC-WTC_000031054
Log sheet detailing sample preparation metrics for Method 608 analysis of WTC samples conducted in December 2001.
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Calibration record for GC/MS instrument using TCLP method, listing standard compounds and response data from November 6, 2001.
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Calibration table listing standard compounds and response values for GCMS analysis dated November 16, 2001.
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Calibration data for GC/MS analysis including naphthalene and phenanthrene standards dated November 6, 2001.
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Calibration data sheet for GC/MS instrument listing standards like naphthalene-d8 used for testing on November 6, 2001.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000087447
Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 4, 2001.
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Calibration data table for GCMS TCLP analysis listing surrogate compounds and response factors from November 2, 2001.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068230
Technical data sheet listing calibration standards and response factors for various polycyclic aromatic hydrocarbons.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069349
Calibration data for GC/MS analysis including naphthalene and phenanthrene standards dated November 8, 2001.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069577
Calibration table data for GCMS analysis dated November 16-21, 2001, listing standard compounds and response values.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068559
Calibration data table for GC/MS instrument used in TCLP analysis, generated on November 5, 2001.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000070089
DEP laboratory report documenting GC/MS results for sample AD25830 analyzed on December 6, 2001.
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