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GCMS analysis results for sample AD26006, Dec 2001

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Laboratory report documenting GCMS analysis of sample AD26006 conducted on December 19-20, 2001.

NYC-WTC_000030836–000030853

Folder label: “GCMS SCAN X 10/31/01 AN 11/21/01

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\DEC1901\26006A.D Vial: 4 Acq On : 20 Dec 2001 9:36 am Operator: GALOS Sample : gc/ms unknown 10/31 Inst : GC/MS Ins Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 20 10:38 2001 Quant Results File: NP112701.RES

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Last Update : Wed Nov 28 15:33:44 2001 Response via : Initial Calibration DataAcq Meth : NP112701

Compound R.T. Qlon Response Cone Unit Qvalue

17) N-Nitrosodi -n-propylamine 13.14 70 2945 N.D. 18) Hexachloroethane 0.00 117 0 N.D. 21) Nitrobenzene 13.54 77 4637 N.D. 22) Isophorone 14.19 82 8812 N.D. 23) 2-Nitrophenol 14.46 139 419 N.D. 24) 2,4-Dimethylphenol 14.72 107 2341 N.D. 25) bis(2-Chloroethoxy)methane 14.89 93 5270 N.D. 26) 2,4-Dichlorophenol 0.00 162 0 N.D. 27) 1,2,4-Trichlorobenzene 15.37 180 2784 N.D. 28) Naphthalene 15.54 128 13137 N.D. 29) Hexachlorobutadiene 16.09 225 936 N.D. 30) 4-Chloro-3-methylphenol 17.42 107 1274 N.D. 34) Hexachlorocyclopentadiene 0.00 237 0 N.D. 35) 2,4,6-Trichlorophenol 0.00 196 0 N.D. 36) 2,4,5-Trichlorophenol 0.00 196 0 N.D. 37) 2-Chloronaphthalene 19.02 162 5944 N.D. 38) Dimethylphthalate 20.13 163 7938 N.D. 39) 2,6-Dinitrotoluene 20.33 165 364 N.D. 40) Acenaphthylene 20.29 152 9044 N.D. 41) Acenaphthene 20.85 153 6649 N.D. 42) 2,4-Dinitrophenol 0.00 184 0 N.D. 43) 4-Nitrophenol 0.00 65 0 N.D. 44) 2,4-Dinitrotoluene 21.52 165 684 N.D. 45) Diethylphthalate 22.24 149 9148 N.D. 46) 4-Chlorophenylphenylether 22.39 204 2920 N.D. 47) Fluorene 22.36 166 7372 N.D. 48) Azobenzen/ 1,2-Diphenylhyd 22.86 77 8745 N.D. 50) 4,6-Dinitro-2-methylphenol 0.00 198 0 N.D. 51) N-Nitrosodiphenylamine 22.78 169 4102 N.D. 52) 4-Bromophenyl-phenylether 23.85 248 1539 N.D. 53) Hexachlorobenzene 24.26 284 916 N.D. 54) Pentachlorophenol 0.00 266 0 N.D. 55) Phenanthrene 25.23 178 10532 N.D. 56) Anthracene 25.23 178 10532 N.D. 57) Di-n-butylphthalate 27.15 149 21980 N.D. 58) Fluoranthene 28.83 202 9284 N.D. 60) 3,3'-Dichlorobenzidine 33.14 252 1095 N.D.

(#) = qualifier out of range (m) = manual integration 26006A.D NP112701.M Thu Dec 20 11:25:54 2001 Page 2

NYC-WTC_000030839

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Gas chromatography-mass spectrometry scan record from late October to November 2001 regarding environmental sample analysis.

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