GCMS analysis results for sample AD26006, Dec 2001

NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\DEC1901\26006A.D Vial: 4 Acq On : 20 Dec 2001 9:36 am Operator: GALOS Sample : gc/ms unknown 10/31 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 20 10:38 2001 Quant Results File: NP112701.RES

Quant Method : G:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator)- Title : 208 625/TCLP calibration table Last Update : Wed Nov 28 15:33:44 2001 Response via : Initial Calibration DataAcq Meth : NP112701

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 11.87 152 1098210 ' 20.00 ng/uL -0.07 19) Naphthalene-d8 15.48 136 4336034 20.00 ng/uL -0.07 31) Acenaphthene-diO 20.76 164 1886702 20.00 ng/uL -0.07 49) Phenanthrene-dlO 25.17 188 2793202 2 0.00 ng/uL -0.08 59) Chrysene-dl2 33.17 240 1895753 20.00 ng/uL -0.08 68) Perylene-dl2 37.26 264 957557 20.00 ng/uL -0.08

System Monitoring Compounds 4) 2-Fluorophenol 8.74 112 1773 0.02 ng/uL 0.00 Spiked Amount 75.000 Range 18 42 Recovery = 0.03%# 5) Phenol-d5 11.17 99 608 0.01 ng/uL 0.04 Spiked Amount 75.000 Range 19 32 Recovery = 0.01%# 6) 2-Chlorophenol-d4 11.39 132 1354 0.02 ng/uL -0.03 Spiked Amount 75.000 Range 34 84 Recovery = 0.03%# 7) 1,2-Dichlorobenzene-d4 12.38 152 1214 0.03 ng/uL -0.08 Spiked Amount 50.000 Range 2 6 73 Recovery = 0.06%# 20) Nitrobenzene-d5 13.48 82 1900 0.02 ng/uL -0.08 Spiked Amount 50.000 Range 55 98 Recovery = 0.04%# 32) 2-Fluorobiphenyl 18.76 172 3265 0.03 ng/uL -0.08 Spiked Amount 50.000 Range 42 78 Recovery = 0.06%# 33) 2,4,6-Tribromophenol 0.00 330 0 0.00 ng/uL Spiked Amount 75.000 Range 45 96 Recovery = 0.00%# 62) Terphenyl-dl4 30.04 244 2959 0.03 ng/uL -0.08 Spiked Amount 50.000 Range 58 98 Recovery = 0.06%#

Target Compounds Qvalue 2) Pyridine 5.14 79 282 N.D. 3) N-nitrosodimethylamine 5.49 74 977 N.D. 8) Phenol 11.21 94 3099 N.D. 9) bis(2-Chloroethyl)ether 11.27 93 4267 N.D. 10) 2-Chlorophenol 11.44 128 1998 N.D. 11) 1,3-Dichlorobenzene 11.77 146 3164 N.D. 12) 1,4-Dichlorobenzene 11.91 146 3594 N.D. 13) 1,2-Dichlorobenzene 12.42 146 3517 N.D. 14) 2-Methylphenol 12.80 108 287 N.D. 15) 2,21-oxybis(1-Chloropropan 12.75 45 9388 N.D. 16) 3&4-Methylphenol 13.25 108 979 N.D.

(#) = qualifier out of range (m) = manual integration 26006A.D NP112701.M Thu Dec 20 11:25:52 2001 Page 1

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