GCMS analysis results for sample AD27232, Dec 2001

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Laboratory report documenting GCMS analysis of sample AD27232 conducted on December 19, 2001.

NYC-WTC_000032847–000032858

Folder label: “GCMS X 11/14/01 A 12/12/01”

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\DEC1201\27232.D Vial: 12 Acq On : 13 Dec 2001 1:18 am Operator : GALOS Sample : gc/ms unknown 11/14 Inst : GC/MS Ins Mise : Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 14 9:35 2001 Quant Results File: NP112701.RES

Quant Method : C:\HPCHEM\1\METHODS\NP112701.M (RTE Integrator) Title : 208 625/TCLP calibration table Last Update : Wed Nov 28 15:33:44 2001 Response via : Initial Calibration DataAcq Meth : NP112701

Compound R.T. Qlon Response Cone Unit Qvalue

17) N-Nitrosodi-n-propylamine 0.00 70 0 N.D. 18) Hexachloroethane 0.00 117 0 N.D. 21) Nitrobenzene 0.00 77 0 N.D. 22) Isophorone 0.00 82 0 N.D. 23) 2-Nitrophenol 0.00 139 0 N.D. 24) 2,4-Dimethylphenol 0.00 107 0 N.D. 25) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 26) 2,4-Dichlorophenol 0.00 162 0 N.D. 27) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 28) Naphthalene 15.52 128 759 N.D. 29) Hexachlorobutadiene 0.00 225 0 N.D. 30) 4-Chloro-3-methylphenol 0.00 107 0 N.D. 34) Hexachlorocyclopentadiene 0.00 237 0 N.D. 35) 2,4,6-Trichlorophenol 0.00 196 0 N.D. 36) 2,4,5-Trichlorophenol 0.00 196 0 N.D. 37) 2-Chloronaphthalene 0.00 162 0 N.D. 38) Dimethylphthalate 0.00 163 0 N.D. 39) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 40) Acenaphthylene 0.00 152 0 N.D. 41) Acenaphthene 0.00 153 0 N.D. 42) 2,4-Dinitrophenol 0.00 184 0 N.D. 43) 4-Nitrophenol 0.00 65 0 N.D. 44) 2,4-Dinitrotoluene 0.00 165 0 N.D. 45) Diethylphthalate 0.00 149 0 N.D. 46) 4-Chlorophenylphenylether 0.00 204 0 N.D. 47) Fluorene 0.00 166 0 N.D. 48) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 50) 4,6-Dinitro-2-methylphenol 0.00 198 0 N.D. 51) N-Nitrosodiphenylamine 0.00 169 0 N.D. 52) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 53) Hexachlorobenzene 0.00 284 0 N.D. 54) Pentachlorophenol 0.00 266 0 N.D. 55) Phenanthrene 0.00 178 0 N.D. 56) Anthracene 0.00 178 0 N.D. 57) Di-n-butylphthalate 27.13 149 3978 N.D. 58) Fluoranthene 0.00 202 0 N.D. 60) 3,31-Dichlorobenzidine 0.00 252 0 N.D.

(#) = qualifier out of range (m) = manual integration 27232.D NP112701.M Fri Dec 14 10:00:40 2001 Page 2

NYC-WTC_000032850

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NYC-WTC_000032850Source: NYC Law Department, mirrored locally

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