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Organic chemical sample results, Nov-Dec 2001

Machine-extracted title · confidence 90%

Analysis results for organic chemicals in sample AD27114 from site 525 collected between November and December 2001.

NYC-WTC_000030450–000030460

Folder label: “525 X 11/14, 11/19, 12/7, 12/17 A 12/1/01 12/3/01 12/18/01 12/19/01

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File C:\MSDCHEM\l\DATA\120601\27114.D Vial: 30 Aca On 7 Dec 2001 3:04 pm Operator: McLean Sample 11/14 sample Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Dec 12 12:38:18 2001 Quant Results File: 120501.RES

Quant Method : C:\MSDCHEM\l\5973N\120501.M (RTE Integrator) Title : Quantitation For Method 525.2 Last Update : Thu Dec 06 10:31:04 2001 Response via : Initial Calibration DataAcq Meth : 120501

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) Acenaphthene-dlO 9) Phenanthrene D-10 18.32 22.65 164 188 4535096 7609074 5.00 ug/L 5.00 ug/L 0.00 0.00 03 20) Chrysene D-12

System Monitoring Compounds 30.43 240 4596252 5.00 ug/L 0.00 2 2) 1,3-Dimethyl-2-nitrobenzen 13.23 134 S07652 3.36 ug/L 0.00 Spiked Amount 5.000 Recovery = 67.20% 19) Triphenyl Phosphate surr 29.70 326 1477276 5.60 ug/L 0.00 Spiked Amount 5.000 Recovery = 112.00% 21) Perylene D-12 surr 34.45 264 2998400 4.65 ug/L 0.00 Spiked Amount 5.000 Recovery = 93.00%

Target Compounds Qvalue 3) Hexachlorocyclopentadiene 0.00 237 0 N.D. 4) Hexachlorobenzene 0.00 284 0 N.D. 5) EPTC 0.00 128 0 N.D. 6) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 7) 2,4-Dinitotoluene 0.00 165 0 N.D. d 8) Molinate 19.08 126 12463 N.D. 10) Simazine 0.00 201 0 N.D. 11) Atrazine 0.00 200 0 N.D. 12) Alachlor 0.00 160 0 N.D. 13) Terbacil 22.78 161 12291 N.D. 14) Acetochlor 0.00 146 0 N.D. 15) Metribuzin 0.00 198 0 N.D. 16) Metolachlor 0.00 162 0 N.D. 17) Butachlor 0.00 160 0 N.D. d 18) 4,4'-DDE 0.00 246 0 N.D. d 22) Bis (2-Ethylhexyl) adipate 29.62 129 21816 0.14 ug/L # 1 23) Bis (2-Ethylhexyl) phthala 31.07 149 417759 0.53 ug/L 92 24) Benzo (a) pyrene 0.00 252 0 N.D. d

(#) = qualifier out of range (m) = manual integration 27114.D 120501.M Wed Dec 12 12:41:44 2001 Page 1

NYC-WTC_000030456

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NYC-WTC_000030456Source: NYC Law Department, mirrored locally

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