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GCMS reference standard results for sample AE11306, May 21, 2002

Machine-extracted title · confidence 95%

Reference standard analysis report for GCMS testing of sample AE11306 conducted on May 21, 2002, verifying instrument performance.

NYC-WTC_000024969–000024976

Folder label: “GCMS X 5/14/02 A 5/21/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\MAY2102\REF1B.D Vial: 18 Acq On : 21 May 2002 5:32 pm Operator: Sample : EXTRACTS/14 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 22 9:04 2002 Quant Results File: GCMS0520.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed May 22 09:03:22 2002 Response via : Initial Calibration DataAcq Meth : GCMS0520

Compound R.T. Qlon Response Cone Unit Qvalue 35) Anthracene 25.72 178 388336 16.52 ug/1 99 36) Di-n-butylphthalate 27.50 149 681792 21.93 ug/1 99 37) Fluoranthene 29.21 202 407146 17.62 ug/1 # 92 3 9) Pyrene 29.88 202 420727 20.87 ug/1 # 91 40) Butylbenzylphthalate 32.02 149 199534 19.37 ug/1 91 41) Benzo(a)anthracene 33.53 228 264860 17.60 ug/1 100 42) Bis(2-ethylhexyl)phthalate 33.81 149 253118 18.69 ug/1 96 43) Chrysene 33.65 228 285435 19.21 ug/1 99 45) Di-n-Octylphthalate 35.55 149 313391 15.65 ug/1 # 95 46) Benzo(b)fluoranthene 36.62 252 216687 16.79 ug/1 97 47) Benzo(k)fluoranthene 36.69 252 239220 17.92 ug/1 97 48) Benzo(a)pyrene 37.60 252 147313 12.30 ug/1 # 96 49) Indeno(1,2,3-cd)pyrene 41.83 276 182190 15.82 ug/1 94 50) Dibenz(a,h)anthracene 41.90 278 154827 16.83 ug/1 # 94 51) Benzo(g,h,i)perylene 43.04 276 157901 17.16 ug/1 # 91

(#) = qualifier out of range (m) = manual integration REFIB.D GCMS0520.M Wed May 22 09:06:17 2002 Page 2

NYC-WTC_000024972

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NYC-WTC_000024972Source: NYC Law Department, mirrored locally

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