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GCMS reference standard analysis, sample AE11604, May 2002

Machine-extracted title · confidence 100%

Reference standard analysis for GCMS method validation on sample AE11604 with compound response values and detection limits.

NYC-WTC_000022634–000022641

Folder label: “GCMS X 5/20/02 A 5/22/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\MAY2102\REFA1.D Vial: 29 Acq On : 22 May 2002 6:08 pm Operator: Sample : EXTRACT5/20 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 24 8:12 2002 Quant Results File: GCMS0520.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon May 20 15:10:30 2002 Response via : Initial Calibration DataAcq Meth : GCMS0520

Compound R.T. Qlon Response Cone Unit Qvalue

35) Anthracene 25.73 178 428443 16.88 ug/1 99 36) Di-n-butylphthalate 27.52 149 713781 21.25 ug/1 99 37) Fluoranthene 29.23 202 449227 17.99 ug/1 95 3 9) Pyrene 29.90 202 458663 20.54 ug/1 94 40) Butylbenzylphthalate 32.04 149 227736 19.96 ug/1 92 41) Benzo(a)anthracene 33.55 228 291896 17.51 ug/1 100 42) Bis(2-ethylhexyl)phthalate 33.83 149 299982 19.99 ug/1 95 43) Chrysene 33.68 228 317037 19.26 ug/1 99 45) Di-n-Octylphthalate 35.58 149 369278 16.47 ug/1 # 98 46) Benzo(b)fluoranthene 36.65 252 241855m 16.75 ug/1 47) Benzo(k)fluoranthene 36.72 252 277106m 18.55 ug/1 48) Benzo(a)pyrene 37.63 252 161272 12.03 ug/1 96 49) Indeno(1,2,3-cd)pyrene 41.89 276 201045 15.60 ug/1 95 50) Dibenz(a,h)anthracene 41.96 278 169643 16.48 ug/1 95 51) Benzo(g,h,i)perylene 43.11 276 178985 17.38 ug/1 94

(#) = qualifier out of range (m) = manual integration REFA1.D GCMS0520.M Fri May 24 08:12:39 2002 Page 2

NYC-WTC_000022637

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NYC-WTC_000022637Source: NYC Law Department, mirrored locally

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