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GCMS reference standard results for sample AE11306, May 21, 2002

Machine-extracted title · confidence 95%

Reference standard analysis report for GCMS testing of sample AE11306 conducted on May 21, 2002, verifying instrument performance.

NYC-WTC_000024969–000024976

Folder label: “GCMS X 5/14/02 A 5/21/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\MAY2102\REF2B.D Vial: 19 Acq On : 21 May 2002 6:32 pm Operator: Sample : EXTRACTS/14 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 22 9:06 2002 Quant Results File: GCMS0520.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed May 22 09:03:22 2002 Response via : Initial Calibration DataAcq Meth : GCMS0520

Compound R.T. Qlon Response Cone Unit Qvalue

35) Anthracene 25.72 178 414547 16.56 ug/1 99 36) Di-n-butylphthalate 27.50 149 721408 21.78 ug/1 99 37) Fluoranthene 29.21 202 435724 17.70 ug/1 # 90 3 9) Pyrene 29.89 202 444037 21.30 ug/1 95 40) Butylbenzylphthalate 32.02 149 214950 20.18 ug/1 92 41) Benzo(a)anthracene 33.53 228 271094 17.42 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.81 149 270237 19.29 ug/1 96 4 3) Chrysene 33.65 228 290432 18.90 ug/1 99 45) Di-n-Octylphthalate 35.55 149 311605 16.46 ug/1 # 95 46) Benzo(b)fluoranthene 36.62 252 208231 17.08 ug/1 98 47) Benzo(k)fluoranthene 36.69 252 231326 18.34 ug/1 97 48) Benzo(a)pyrene 37.59 252 138322 12.22 ug/1 # 94 49) Indeno(1,2,3-cd)pyrene 41.83 276 160983 14.80 ug/1 93 50) Dibenz(a,h)anthracene 41.90 278 136363 15.69 ug/1 # 94 51) Benzo(g,h,i)perylene 43.03 276 141415 16.26 ug/1 94

(#) = qualifier out of range (m) = manual integration REF2B.D GCMS0520.M Wed May 22 09:08:16 2002 Page 2

NYC-WTC_000024975

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NYC-WTC_000024975Source: NYC Law Department, mirrored locally

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