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GCMS reference standard analysis, sample AE11604, May 2002

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Reference standard analysis for GCMS method validation on sample AE11604 with compound response values and detection limits.

NYC-WTC_000022634–000022641

Folder label: “GCMS X 5/20/02 A 5/22/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\MAY2102\REFA2.D Vial: 30 Acq On : 22 May 2002 7:07 pm Operator: Sample : EXTRACT5/20 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 24 8:12 2002 Quant Results File: GCMS0520.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon May 20 15:10:30 2002 Response via : Initial Calibration DataAcq Meth : GCMS0520

Compound R.T. Qlon Response Cone Unit Qvalue 35) Anthracene 25.72 178 442767 17.35 ug/1 100 36) Di-n-butylphthalate 27.50 149 746275 22.11 ug/1 99 37) Fluoranthene 29.21 202 470144 18.74 ug/1 # 92 3 9) Pyrene 29.89 202 486932 21.16 ug/1 95 40) Butylbenzylphthalate 32.02 149 239739 20.39 ug/1 94 41) Benzo(a)anthracene 33.53 228 314460 18.30 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.81 149 307719 19.90 ug/1 97 43) Chrysene 33.65 228 341238 20.11 ug/1 99 45) Di-n-Octylphthalate 35.55 149 379126 16.64 ug/1 # 96 46) Benzo(b)fluoranthene 36.62 252 257429 17.54 ug/1 98 4 7) Benzo(k)fluoranthene 36.69 252 283053 18.65 ug/1 98 48) Benzo(a)pyrene 37.59 252 169941 12.48 ug/1 # 95 49) Indeno(1,2,3-cd)pyrene 41.82 276 199604 15.24 ug/1 95 50) Dibenz(a,h)anthracene 41.90 278 173693 16.60 ug/1 # 94 51) Benzo(g,h,i)perylene 43.04 276 177568 16.97 ug/1 93

(#) = qualifier out of range (m) = manual integration REFA2.D GCMS 0 52 0.M Fri May 24 08:18:01 2002 Page 2

NYC-WTC_000022640

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NYC-WTC_000022640Source: NYC Law Department, mirrored locally

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