GCMS reference standard analysis, sample AE11604, May 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\MAY2102\REFA2.D Vial: 30 Acq On : 22 May 2002 7:07 pm Operator: Sample : EXTRACTS/20 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 24 8:12 2002 Quant Results File: GCMS0520.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon May 20 15:10:30 2002 Response via : Initial Calibration DataAcq Meth : GCMS0520

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.14 152 402802 40.00 ug/1 0.00 10) Naphthalene-d8 15.78 136 1582036 40.00 ug/1 -0.02 17) Acenaphthene-diO 21.08 164 758656 40.00 ug/1 0.00 30) Phenanthrene-diO 25.53 188 1028433 40.00 ug/1 0.00 38) Chrysene-dl2 33.58 240 627747 40.00 ug/1 -0.03 44) Perylene-dl2 37.79 264 393739 40.00 ug/1 -0.02

System Monitoring Compounds 28) TCMX 23.23 209 151214 39.66 ug/L 0.00 Spiked Amount 40.000 Recovery 99.15%

Target Compounds Qvalue 2) N-nitrosodimethylamine 5.80 74 143382 11.86 ug/1 95 3) bis(2-Chloroethyl)ether 11.54 93 288902 18.04 ug/1 97 4) 1,3-Dichlorobenzene 12.04 146 211272 16.30 ug/1 97 5) 1,4-Dichlorobenzene 12.18 146 223255 15.72 ug/1 98 6) 1,2-Dichlorobenzene 12.70 146 216233 17.57 ug/1 98 7) 2,2'-oxybi s(1-Chloropropan 13.03 45 647286 17.86 ug/1 99 8) N-Nitrosodi-n-propylamine 13.41 70 197060 17.33 ug/1 97 9) Hexachloroethane 13.55 117 73820 12.17 ug/1 # 83 11) Nitrobenzene 13.82 77 256667 18.67 ug/1 94 12) Isophorone 14.47 82 567678 20.85 ug/1 100 13) bis(2-Chloroethoxy)methane 15.15 93 346144 18.97 ug/1 99 14) 1,2,4-Trichlorobenzene 15.67 180 161959 16.39 ug/1 97 15) Naphthalene 15.83 128 712123 19.94 ug/1 99 16) Hexachlorobutadiene 16.38 225 60472 12.65 ug/1 98 18) Hexachlorocyclopentadiene 18.58 237 6768 2.20 ug/1 91 19) 2-Chloronaphthalene 19.34 162 351772 20.80 ug/1 96 20) Dimethylphthalate 20.44 163 426651 20.05 ug/1 99 21) 2,6-Dinitrotoluene 20.65 165 82319 18.58 ug/1 94 22) Acenaphthylene 20.61 152 555339 17.92 ug/1 100 23) Acenaphthene 21.17 153 380451 20.55 ug/1 99 24) 2,4-Dinitrotoluene 21.81 165 96465 19.86 ug/1 93 25) Diethylphthalate 22.57 149 432974 22.02 ug/1 96 26) 4-Chlorophenylphenylether 22.72 204 179540 18.26 ug/1 95 27) Fluorene 22.69 166 390017 20.78 ug/1 99 29) Azobenzene 23.18 77 506263 17.87 ug/L 96 31) N-Nitrosodiphenylamine 23.11 168 125567 18.53 ug/1 # 92 32) 4-Bromophenylphenylether 24.19 248 97067 18.08 ug/1 94 33) Hexachlorobenzene 24.62 284 107828 18.72 ug/1 # 90 3 4) Phenanthrene 25.59 178 508258 20.49 ug/1 100

(#) = qualifier out of range (m) = manual integration REFA2.D GCMS0520.M Fri May 24 08:18:00 2002 Page 1

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