GCMS analysis results for sample AE10852, May 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\1\DATA\MAY1502\10852.D Vial: 7 Acq On : 15 May 2002 7:56 pm Operator: Sample : GC/MS SCAN 5/10 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 2 1-Pentanamine Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 9.94 0.71 ug/1 38545 1,4-Dichlorobenzene-d4 12.16 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1-Pentanamine 87 C5H13N 000110-58-7 12 2 3-Pyrrolidinol 87 C4H9NO 040499-83-0 9 3 Acetic acid, 1-methylpropyl ester 116 C6H1202 000105-46-4 9 4 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 9 Abundance Scan 535 (9.940 min): 10852.D (-) m/z 43.05 100.00% 43

5000

58 ■ i 1 ■ ■ ■ i ■ 87 । 98 9.60 9.80 10.00 10.20 TTTTTTTTTTTTTTTTTTT . THTTTT m/ Z 58.00 21.17% m/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #62890: 1-Pentanamine 33

5000 —AAA— 9.60 9.80 10.00 10.20 m/ z 87.05 14.72% I' ■'11" ■ ■ i ■ ■ ■' i'1 41 55 73 HTTITTTTT+HHTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTTT 87 m/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #752:3-Pyrrolidinol 43 ........ |......... ' 1 i ■ ■ ■ 1 1 • 1 ' ■ i 1 1 1 1 I 1 1 1 1 1 1 9.60 9.80 10.00 10.20 5000 m/z 59.10 11.10%

57 87 68 '1 ■ ■ i' ■1' i ■■" i'‘" i' ■'' i ■ ■ ■■ i1■'■i mHH+H I’’ m/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #64338: Acetic acid, 1-methylpropyl ester ■ ■ i 1 43 9.60 9.80 10.00 10.20 m/ z 41.05 10.76% 5000

56 87 27 15 27 , 1 <11111111 ‘1 *11>*>>[■1111111111111111 ! 11111111111 .1 61 73 1 101 1111111111111111I111111111111111111111 [ 111111111111111

m/z—> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 9.60 9.80 10.00 10.20

10852.D GCMS0510.M Fri May 17 10:00:02 2002 Page 2

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