GCMS analysis results for sample AE11378, May 28, 2002

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\HPCHEM\1\DATA\MAY2102\11377.D Vial: 26 Acq On : 22 May 2002 1:24 am Operator: Sample : EXTRACTS/14 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 2 Acetone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 9.92 0.53 ug/1 34896 1,4-Dichlorobenzene-d4 12.14 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetone 58 C3H60 000067-64-1 9 2 3-Pyrrolidinol 87 C4H9NO 040499-83-0 9 3 l-Pentanamine 87 C5H13N 000110-58-7 9 4 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 9 Abundance Scan 532 (9,920 min): 11377. D (-) m/z 43.05 100.00% 43

5000

58 11011 | I | | | in- | | | I 87 Ipl. 98 9.60 9.80 10.00 10.20 ti'i " I" " III Lim I."1 + H m/ z 58.10 21.79% m/z—> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #62322: Acetone 43

5000 58 9.60 m/z .y. ' 1 i 1 1 • ' i 1 ; 1 ' 1 1 1 ■ ' i 9.80 10,00 10.20 87.05 15.80% 27

m/z—> -H * 11" 11 r " 11" 11 r ■ " r 11111111111111111111111111 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #752:3-Pyrrolidinol 43 1 । 1 1 1 1 । 1 ‘ ■ । 1 ■ 1 1 । 9.60 9.80 10,00 10,20 5000 m/z 41.15 13.38% 87 57 68 " " i" " i" " i ■'" i ■ ‘‘ i i " " i " " r ' " i " ' ■ i ■ " ' i' ■111 ■1 ■ ■ i ‘ ' m/z-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance 33 #62890:1-Pentanamine AQAAMAA 9.60 —MMA—A,M 9.80 10.00 10.20 m/ z 59.10 12.00% 5000

1 41 45 55 87 73 "I—T'l" 111 > 11111111111 > 11 TT100TOong" 1" i1''' r 1111" " I" " I " m/z-> 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 9.60 9.80 10.00 10.20

11377.D GCMS0520.M Wed May 22 09:22:08 2002 Page 2

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