GCMS calibration table data, sample AE09679, May 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\MAY0 602\9679.D Vial: 22 Acq On 7 May 2002 12:51 pm Operator: Sample GC/MS SCAN 4/25 Inst : 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 8.16 11.62 ug/1 943856 1,4-Dichlorobenzene-d4 12.19 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H1202 000123-42-2 64 2 CH2=C H2C (O) OCH3 100 C5H802 003724-55-8 9 3 Aceti acid, 1,1-dimethylethyl este 116 C6H1202 000540-88-5 9 4 Aceto 58 C3H60 000067-64-1 7 Abundance Scan 341 (8.162 min): 9679.D (-) m/z 43.05 100.00% 43

5000 59

101 7.80 8.00 8.20 8.40 8.60 v. 10. ....2II—30... 38,1, + 531 69 83 !■ ■ ■ ' i • ' ■ ‘ i ''' ■ ■ i ■ 1 '‘’"I ' 1 1 1 1 1 m/z 59.10 42.82% m/z-> 20 40 50 60 70 80 90 100 110 Abundance #64274:2-Pentanone, 4-hydroxy-4-methyl- 43

5000 ■ ■ i 1 1 ■ ■ i 1 ‘ ‘ ■ i 1*. । . 59 7.80 8.00 8.20 8.40 8.60 m/z 58.10 16.87%

niz-> Abundance 10 20 27 1 I 30 H 40 +49+ 50 1 60 70 #1448: CH2=CHCH2C(O)OCH3 80 83 . । . . . . i .' ‘ । . 90 +. 101 100 110 43 - 7.80 8.00 8.20 8.40 8.60 5000 m/z 101.15 13.85%

• ■ । 111 > • 1 • > • •58 * > i l 72 > • ■ i I > • • j 1 ■ • 1 । • * 100 mfz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #3292: Acetic acid, 1,1-dimethylethyl ester 43 7.80 8.00 8.20 8.40 8.60 m/z 41.10 6.84% 5000 57 101 15 27 i 1 P1’rr1 [2*1 1477174/7p* r-j". mlz~> 1 ' I ■ ■ ‘ 10 20 ' 1 1 I ' ' 30 1 • i 1 40 11Bol 60 1i ‘ ■ ■ ■ i' ■ ■ • i ’1 1 1 i 1 ' 1 rr' ‘ 1 1 i 1 70 80 90 100 110 7.80 8.00 8.20 8.40 8.60

9679.D GCMS0501.M Thu May 09 11:25:39 2002 Page 1

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