GC/MS results for unknown compounds and surrogates, sample AE10985, May

NYC 9/11 Public Portal Document Library Search Compound Report Data File : C:\MSDCHEM\l\DATA\051402\10985.D Vial: 14 Acq On : 15 May 2002 12:06 am Operator: Mclean Sample : 5/10 kb Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\1\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L Peak Number 3 Propane, 2-(ethenyloxy)- Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 3.70 0.24 ug/L 187274 1,4-Dichlorobenzene-d4 9.93 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Propane, 2-(ethenyloxy) - 86 C5H10O 000926-65-8 9/ 2 2-Butanone, 3-methyl- 86 C5H10O 000563-80-4 9 3 Pentane, 2-bromo-2-methyl- 164 C6H13Br 004283-80-1 2 4 Pentane, 2-bromo-4-methyl- 164 C6H13Br 030310-22/6 2 Abundance Scan 105 (3.696 min): 10985.D (-97) (-) m/z 43.10 100.00% 43

5000 -/A 151 86

60 3.40 3.60 3.80 4.00 0- —PmPP mPT ------- m/z 41.10 73.81% m/z-> 0 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #4753: Propane, 2-(ethenyloxy)- 43

5000 27 "WAalyaal 3,40 3.60 3.80 4.00 15 86 m/z 49.10 47.14%

m/z-> 0- "Z 2 — 7 11‘‘‘‘114‘1144+/1‘‘A/1*1I‘I‘‘A+1‘‘‘‘I‘l‘+1‘’ 10 20 30 40 50 60 70 80 90 100 1'10 120 130 140 150 160 170 "Mww"s Abundance #109357: 2-Butanone, 3-methyl- 43 3.40 3.60 3.80 4.00 5000 m/z 85.95 26.31%

0- H 15 Hl57 27 71 i 86

1...... 'I'....... ... "Mapy/Hohoynn m/z-> 0 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 Abundance #109354: Pentane, 2-bromo-2-methyl- 43 3.40 3.60 3.80 4.00 m/z 51.10 25.49% 5000 27 69 85 "MhausyuHMaaahpy 15 55

m/z-> 0 -Iml +77+4+93. 107 121 135 164 0 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 ' i" "i'" ■ i ‘■ " i" i ■ • ■ ■ i'' •' i" " i ■ ■ 3.40 3.60 3.80 4.00

10985.D 050102.M Thu May 16 14:42:31 2002 Page 6

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