GCMS sample analysis results, AE11902, June 3, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\MSDCHEM\1\DATA\052202\11902.D Vial: 9 Acq On : 22 May 2002 8:20 pm Operator: Mclean Sample : 5/21 ad Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e Quant Method : C:\MSDCHEM\I\METHODS\050102.M (Chemstation Integrator) Title : 508 Modified GC/MS scan Library : C:\DATABASE\NIST98.L ********************************************************************* Peak Number 3 1,1,2-Trifluoroethane Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 3.83 2.57 ug/L 1653150 1,4-Dichlorobenzene-d4 9.90 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,1,2-Trifluoroethane 84 C2H3F3 000430-66-0 4 2 2-Butyne-1,4-diol, diformate 142 C6H604 036677-73-3 A 3 Propiolonitrile 51 C3HN 001070-71-9 3 4 Methane, chloro- 50 CH3C1 000074-87/3 3 Abundance Scan 128 (3.831 min): 11902.D (-126) (-) m/z 51.10 0.00% 51

36 5000 58 86

44 3.40 3.60 3.80 4.00 4.20 - Ot ■ ‘ i 1 ■ ■ 1 i ■ ■ ■ ■ i • ■ - i ■ ■ ■ ■ i 1 m/z 36.10 60.00% nz-> 10 20 30 40 50 70 80 90 100 110 120 130 Abundance #12369:1,1,2-Trifluoroethane 51 wporlyphts. 5000 33 45 3.40 3.60 3.80 4.00 4.20 65 m/z 50.05 50.48% .... 19 26 .... 1. miz-> Abundance Ot I 1 |T > , l'| I t’lu I1!1, 1 , I rel i I1 -t-r-r • ।'''1 10 20 29 30 40 39 50 60 ,1 70 #381:2-Butyne-1,4-diol, diformate 80 84 90 100 110 120 130 wMMMAplu 3.40 3.60 3.80 4.00 4.20 5000 51 m/z 86.00 47.24% 68 18 ,58

niz-> 0- 111 '' " ' 10 20 —30 1144441 40 50 97 105 113 444—+ -1-76—86 , . T 60 70 80 125 90 100 110 120 130 Abundance #12371: Propiolonitrile 51 3.40 3.60 3.80 4.00 4.20 m/z 58.10 44.38% 5000

12 4 0 25 2 38 0- ,,, +18 .Hl-, 32 M- m 1 ■ ■ ■ । ■1 ■' । ■ ■ ■ • । ■ ■ ■ ■ । ■ ■ ■ ■ । ■ ■ ■ • । ■ ■ ■ ■ । * ■ ■ ■ । •

n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 3.40 3.60 3.80 4.00 4.20

11902.D 052202.M Tue May 28 12:06:35 2002 Page 6

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