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GCMS results for sample AE10062, May 2002

Machine-extracted title · confidence 95%

Laboratory report of GCMS analysis for sample AE10062 conducted on May 23, 2002, showing surrogate recovery data.

NYC-WTC_000023684–000023690

Folder label: “GCMS X 5/9/02 A 5/20/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\MAY0302\10062.D Vial: 35 Acq On 5 May 2002 1:20 am Operator: Sample GC/MS SCAN 4/26 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 7 11:53 2002 Quant Results File: GCMS0501.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) - N Title : 209 625/TCLP calibration table y Last Update : Wed May 01 10:40:31 2002 P Response via : Initial Calibration XC DataAcq Meth : GCMS0501 WW 0

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.19 152 467327 40.00 ug/1 -0.02 10) Naphthalene-d8 15.82 136 1705404 40.00 ug/1 -0.03 17) Acenaphthene-diO 21.14 164 924025 40.00 ug/1 -0.01 30) Phenanthrene-diO 25.57 188 1287669 40.00 ug/1 -0.02 38) Chrysene-dl2 33.64 240 839977 40.00 ug/1 -0.03 44) Perylene-dl2 37.86 264 554936 40.00 ug/1 -0.02

System Monitoring Compounds 28) TCMX 23.27 209 19951 4.44 ug/L -0.02 Spiked Amount 10.000 Recovery = 44.40%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2' - oxybi s (1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0 00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.88 128 180 N.D. 16) Hexachiorobut adi ene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.61 149 787 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 29) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 31) N-Nitrosodiphenylamine 0.00 168 0 N.D. 32) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 33) Hexachlorobenzene 0.00 284 0 N.D. 34) Phenanthrene 25.57 178 350 N.D.

(#) = qualifier out of range (m) = manual integration 10062.D GCMS0501.M Tue May 07 11:53:34 2002 Page 1

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