GC/MS reference analysis results, sample AE09676, May 20-21 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\1\DATA\MAY2002\REF2.D Vial: 8 Acq On : 20 May 2002 2:04 pm Operator: Sample : EXTRACTED 5/9 Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 20 15:22 2002 <Quant Results File: GCMS0520.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon May 20 15:10:30 2002 Response via : Initial Calibration DataAcq Meth : GCMS0520

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.14 152 336166 40.00 ug/1 0.00 10) Naphthalene-d8 15.78 136 1338423 40.00 ug/1 -0.01 17) Acenaphthene-diO 21.08 164 626927 40.00 ug/1 0.00 30) Phenanthrene-diO 25.52 188 848441 40.00 ug/1 -0.01 38) Chrysene-dl2 33.57 240 482911 40.00 ug/1 -0.03 44) Perylene-dl2 37.79 264 292568 40.00 ug/1 -0.01

System Monitoring Compounds 28) TCMX 23.23 209 124019 39.36 ug/L 0.00 Spiked Amount 40.000 Recovery 98.40%

Target Compounds Qvalue 2) N-nitrosodimethylamine 5.80 74 121856 12.07 ug/1 90 3) bis(2-Chloroethyl)ether 11.54 93 229869 17.20 ug/1 99 4) 1,3-Dichlorobenzene 12.04 146 166564 15.40 ug/1 98 5) 1,4-Dichlorobenzene 12.19 146 174959 14.76 ug/1 99 6) 1,2-Dichlorobenzene 12.70 146 169414 16.50 ug/1 99 7) 2,2'-oxybis(1-Chloropropan 13.03 45 567378 18.76 ug/1 98 8) N-Nitrosodi-n-propylamine 13.41 70 172964 18.22 ug/1 93 9) Hexachloroethane 13.55 117 60224 11.90 ug/1 84 11) Nitrobenzene 13.83 77 207261 17.82 ug/1 93 12) Isophorone 14.47 82 467378 20.29 ug/1 99 13) bis(2-Chloroethoxy)methane 15,. 16 93 272715 17.66 ug/1 99 14) 1,2,4-Trichlorobenzene 15.67 180 131917 15.78 ug/1 99 15) Naphthalene 15.83 128 561396 18.58 ug/1 99 16) HexachlOrobutadiene 16.38 225 53316 13.18 ug/1 99 18) Hexachlorocyclopentadiene 18.57 237 10362 4.08 ug/1 95 19) 2-Chloronaphthalene 19.33 162 276724 19.80 ug/1 96 20) Dimethylphthalate 20.43 163 332682 18.91 ug/1 100 21) 2,6-Dinitrotoluene 20.64 165 63704 17.40 ug/1 # 88 22) Acenaphthylene 20.61 152 427581 16.70 ug/1 99 2 3) Acenaphthene 21.18 153 295045 19.29 ug/1 99 24) 2,4-Dinitrotoluene 21.82 165 73837 18.40 ug/1 93 25) Diethylphthalate 22.57 149 336827 20.72 ug/1 98 26) 4-Chlorophenylphenylether 22.72 204 149406 18.39 ug/1 99 27) Fluorene 22.70 166 302505 19.51 ug/1 100 29) Azobenzene 23.18 77 407236 17.39 ug/L 94 31) N-Nitrosodiphenylamine 23.11 168 95213 17.03 ug/1 # 89 32) 4-Bromophenylphenylether 24.18 248 79738 18.00 ug/1 97 33) Hexachlorobenzene 24.61 284 90194 18.98 ug/1 # 92 3 4) Phenanthrene 25.58 178 390006 19.06 ug/1 100

(#) = qualifier out of range (m) = manual integration REF2.D GCMS0520.M Mon May 20 15:23:21 2002 Page 1

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