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GC/MS calibration data, May 20-21 2002

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Laboratory report showing GC/MS calibration data for volatile organic compounds analyzed on May 20-21, 2002.

NYC-WTC_000023662–000023665

Folder label: “GCMS X 5/9/02 A 5/20/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\MAY2 0 02\CALIO OB.D Vial: 5 Acq On 20 May 2002 12:06 pm Operator: Sample Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 20 14:59 2002 Quant Results File: GCMS0520.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon May 20 11:18:45 2002 Response via : Initial Calibration DataAcq Meth : GCMS0510

Compound R.T. Qlon Response Cone Unit Qvalue 35) Anthracene 25.76 178 5031087 191.00 ug/1 99 36) Di-n-butylphthalate 27.53 149 6609523 189.66 ug/1 99 37) Fluoranthene 29.25 202 5070713 195.75 ug/1 # 92 3 9) Pyrene 29.92 202 4723129 183.77 ug/1 92 40) Butylbenzylphthalate 32.06 149 2599239 197.93 ug/1 99 41) Benzo(a)anthracene 33.56 228 3797775 197.94 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.83 149 3428025 198.53 ug/1 98 43) Chrysene 33.70 228 3664476 193.43 ug/1 98 45) Di-n-Octylphthalate 35.57 149 5262497 229.54 ug/1 # 95 46) Benzo(b)fluoranthene 36.67 252 3236746 219.19 ug/1 97 47) Benzo(k)fluoranthene 36.75 252 3149877 206.19 ug/1 98 48) Benzo(a)pyrene 37.66 252 2833270 206.71 ug/1 97 49) Indeno(1,2,3-cd)pyrene 41.92 276 2580190 195.81 ug/1 95 5 0) Dibenz(a,h)anthracene 41.99 278 2075612 197.16 ug/1 97 51) Benzo(g,h,i)perylene 43.16 276 1982665 188.23 ug/1 95

(#) = qualifier out of range (m) = manual integration CAL100B.D GCMS0520.M Mon May 20 15:01:17 2002 Page 2

NYC-WTC_000023664

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NYC-WTC_000023664Source: NYC Law Department, mirrored locally

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