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GCMS calibration results for sample AE10851, May 2002

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Laboratory report displaying GCMS calibration results for sample AE10851 on May 15, 2002, including response factors for target compounds.

NYC-WTC_000024197–000024208

Folder label: “GCMS X 5/10/02 A 5/15/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) Data File C:\HPCHEM\1\DATA\MAY15 0 2\CAL4 0.D Vial: 2 Acq On 15 May 2002 9:34 am Operator: Sample Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 15 15:28 2002 Quant Results File: GCMS0510.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed May 15 14:56:50 2002 Response via : Initial Calibration DataAcq Meth : GCMS0510

Compound R.T. Qlon Response Cone Unit Qvalue 35) Anthracene 25.75 178 1502095 39.73 ug/1 99 36) Di-n-butylphthalate 27.53 149 2051115 43.74 ug/1 99 37) Fluoranthene 29.25 202 1561016 43.01 ug/1 93 3 9) Pyrene 29.92 202 1464097 43.49 ug/1 92 40) Butylbenzylphthalate 32.06 149 760788 44.40 ug/1 95 41) Benzo(a)anthracene 33.56 228 1114161 42.92 ug/1 100 42) Bis(2-ethylhexyl)phthalate 33.84 149 930970 40.97 ug/1 97 43) Chrysene 33.69 228 1090551 42.08 ug/1 100 45) Di-n-Octylphthalate 35.58 149 1336879 45.75 ug/1 # 91 46) Benzo(b)fluoranthene 36.67 252 883657 44.08 ug/1 97 47) Benzo(k)fluoranthene 36.74 252 944479 44.51 ug/1 98 48) Benzo(a)pyrene 37.65 252 780152 43.06 ug/1 # 96 49) Indeno(1,2,3-cd)pyrene 41.93 276 708343m 41.16 ug/1 5 0) Dibenz(a,h)anthracene 41.99 278 565584 41.25 ug/1 96 51) Benzo(g,h,i)perylene 43.16 276 571863 41.54 ug/1 94

(#) = qualifier out of range (m) = manual integration CAL40.D GCMS0510.M Wed May 15 15:28:55 2002 Page 2

NYC-WTC_000024199

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NYC-WTC_000024199Source: NYC Law Department, mirrored locally

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