GC/MS calibration data, May 20-21 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C: \HPCHEM\1\DATA\MAY2 002 \CAL10OB . D Vial: 5 Acq On Sample 20 May 2002 12:06 pm 0° - Operator: Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 20 14:59 2002 Quant Results File: GCMS0520.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Mon May 20 11:18:45 2002 Response via : Initial Calibration DataAcq Meth : GCMS0510

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.15 152 391753 40.00 ug/1 0.00 10) Naphthalene-d8 15.79 136 1560453 40.00 ug/1 0.00 17) Acenaphthene-diO 21.09 164 729683 40.00 ug/1 0.00 30) Phenanthrene-diO 25.53 188 1061684 40.00 ug/1 0.00 38) Chrysene-dl2 33.61 240 700965 40.00 ug/1 0.00 44) Perylene-dl2 37.80 264 396256 40.00 ug/1 0.00

System Monitoring Compounds 28) TCMX 23.23 209 35619 9.71 ug/L 0.00 Spiked Amount 10.000 Recovery = 97.10%

Target Compounds /4o-24o Qvalue 2) N-nitrosodimethylamine 5.83 74 2307218 196.18 ug/1 92 3) bis(2-Chloroethyl)ether 11.56 93 2988431 191.84 ug/1 98 4) 1,3-Dichlorobenzene 12.05 146 2449564 194.31 ug/1 99 5) 1,4-Dichlorobenzene 12.20 146 2680474 194.05 ug/1 97 6) 1,2-Dichlorobenzene 12.71 146 2340951 195.61 ug/1 99 7) 2,2'-oxybis(1-Chloropropan 13.03 45 6566496 186.32 ug/1 98 8) N-Nitrosodi-n-propylamine 13.45 70 2142973 193.73 ug/1 94 9) Hexachloroethane 13.56 117 1154139 195.69 ug/1 87 11) Nitrobenzene 13.85 77 2752952 202.99 ug/1 92 12) Isophorone 14.49 82 5104629 190.07 ug/1 98 13) bis(2-Chloroethoxy)methane 15-. 19 93 3425652 190.29 ug/1 99 14) 1,2,4-Trichlorobenzene 15.68 180 1891609 194.07 ug/1 97 15) Naphthalene 15.87 128 6578102 186.70 ug/1 99 16) Hexachlorobutadiene 16.39 225 914433 193.87 ug/1 99 18) Hexachlorocyclopentadiene 18.59 237 813025 274.76 ug/1 99 19) 2-Chloronaphthalene 19.36 162 3190040 196.14 ug/1 96 20) Dimethylphthalate 20.48 163 4018332 196.29 ug/1 99 21) 2,6-Dinitrotoluene 20.70 165 973968 228.55 ug/1 96 22) Acenaphthylene 20.64 152 5710162 191.62 ug/1 99 23) Acenaphthene 21.21 153 3380561 189.87 ug/1 98 24) 2,4-Dinitrotoluene 21.86 165 1103154 236.16 ug/1 98 25) Diethylphthalate 22.61 149 3697461 195.47 ug/1 99 26) 4-Chlorophenylphenylether 22.75 204 1787466 189.03 ug/1 99 27) Fluorene 22.73 166 3419029 189.41 ug/1 99 29) Azobenzene 23.22 77 5447829 199.92 ug/L 97 31) N-Nitrosodiphenylamine 23.14 168 1179582 168.60 ug/1 # 90 32) 4-Bromophenylphenylether 24.20 248 1079839 194.82 ug/1 100 33) Hexachlorobenzene 24.64 284 1177121 197.96 ug/1 96 34) Phenanthrene 25.63 178 4868989 190.17 ug/1 99

(#) = qualifier out of range (m) = manual integration CALIOOB.D GCMS0520.M Mon May 20 15:01:16 2002 Page 1

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