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GCMS calibration results for sample AE11604, May 2002

Machine-extracted title · confidence 100%

Reference standard analysis for GCMS method validation on sample AE11604 with compound response values and detection limits.

NYC-WTC_000022630–000022633

Folder label: “GCMS X 5/20/02 A 5/22/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File C:\HPCHEM\1\DATA\MAY2102\CAL4 0B.D Vial: 2 Acq On 21 May 2002 3:34 pm Operator: Sample Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 24 8:39 2002 Quant Results File: GCMS0520.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0520.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri May 24 08:38:50 2002 Response via : Initial Calibration DataAcq Meth : GCMS0520

Compound R.T. Qlon Response Cone Unit Qvalue 35) Anthracene 25.73 178 1104440 41.83 ug/1 100 36) Di-n-butylphthalate 27.50 149 1509401 43.21 ug/1 99 37) Fluoranthene 29.22 202 1058439 40.77 ug/1 94 3 9) Pyrene 29.89 202 984473 39.58 ug/1 92 40) Butylbenzylphthalate 32.03 149 543852 42.80 ug/1 96 41) Benzo(a)anthracene 33.53 228 725856 39.10 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.81 149 735286 44.00 ug/1 96 43) Chrysene 33.66 228 735437 40.12 ug/1 100 45) Di-n-Octylphthalate 35.55 149 1076625 43.49 ug/1 # 96 46) Benzo(b)fluoranthene 36.63 252 616019 38.63 ug/1 98 47) Benzo(k)fluoranthene 36.70 252 650509 39.43 ug/1 97 48) Benzo(a)pyrene 37.60 252 579644 39.16 ug/1 96 49) Indeno(1,2,3-cd)pyrene 41.85 276 549278 38.60 ug/1 95 50) Dibenz(a,h)anthracene 41.91 278 430694 37.89 ug/1 97 51) Benzo(g,h,i)perylene 43.06 276 443361 38.98 ug/1 95

(#) = qualifier out of range (m) = manual integration CAL40B.D GCMS0520.M Fri May 24 08:40:15 2002 Page 2

NYC-WTC_000022632

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NYC-WTC_000022632Source: NYC Law Department, mirrored locally

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