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GCMS calibration table for TCLP analysis, May 2002

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Calibration table and response data for TCLP volatile organic analysis using Method GCMS0501 on sample AE09520 analyzed in May 2002.

NYC-WTC_000023363–000023371

Folder label: “GCMS X 5/8/02 A 5/9/02

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NYC 9/11 Public Portal Document Quantitation Report (QT Reviewed) Data File C:\HPCHEM\l\DATA\MAY0302\9520.D Vial: 21 Acq On 4 May 2002 9:41 am Operator: Sample GC/MS SCAN 4/22 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: May 7 9:29 2002 Quant Results File: GCMS0501.RES Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed May 01 10:40:31 2002 Response via : Initial Calibration DataAcq Meth : GCMS0501

Compound R.T. Qlon Response Cone Unit Qvalue 35) Anthracene 25.57 178 393 N.D. 36) Di-n-butylphthalate 27.55 149 8595 N.D. 37) Fluoranthene 0.00 202 0 N.D. 3 9) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 33.63 228 1990 N.D. 42) Bis(2-ethylhexyl)phthalate 33.86 149 1978 N.D. 43) Chrysene 33.63 228 1990 N.D. 45) Di-n-Octylphthalate 0.00 149 0 N.D. 46) Benzo(b)fluoranthene 0.00 252 0 N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. 48) Benzo(a)pyrene 37.87 252 2026 N.D. 49) Indeno(l,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 9520.D GCMS0501.M Tue May 07 09:30:15 2002 Page 2

NYC-WTC_000023364

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NYC-WTC_000023364Source: NYC Law Department, mirrored locally

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