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GCMS analysis results for sample AE08485, May 2002

Machine-extracted title · confidence 90%

Laboratory report showing GCMS analysis of sample AE08485 conducted on May 16, 2002.

NYC-WTC_000023273–000023282

Folder label: “GCMS X 5/8/02 A 5/9/02

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Scanned page image, NYC-WTC_000023281
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\MAY0902\8485.D Vial: 11 Acq On : 10 May 2002 12:12 am Operator: Sample : GC/MS SCAN 5/8 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0510.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 14.80 1.52 ug/1 137181 Naphthalene-d8 15.82 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopen siloxane, decamethyl- 370 C10H3005Si5 000541-02-6/80 2 3,4-Dih roxybenzyl alcohol,tris(tr 356 C16H3203Si3 068595-79-9 38 3 Noradr .aline, tetra-TMS 457 C20H43NO3Si4 000000-00-0 37 4 Benze ethanamine, N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 37 Abundance Scan 1065 (14.798 min): 8485.D (-) m/z 73.10 100.00% 73

5000 267 355

45 14.40 14.60 14.80 15.00 15.20

m/z-> I 108 133154 I 193 TWTTTTTTTTTTITTHTTTTT I"' 'I 237 , 40 60 80 100120140160180200220240260280300320340360380400420440 —?3lmmH m/z 267.05 35.00%| Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 / 5000 14.40 14.60 14.80 15.00 15.20 m/z 355.10 34.54%| 207 i" ■ ''i" " r "11" " i"1 ■ r " ■ r ■" r ■" i " i T—im"p 323 , miz-> 40 60 80 100120140160180200220240260280300320340360380400420440 Abundance #49868:3,4-Dihydroxybenzyl alcohol,tris(trimethylsilyl)- 73

14.40 14.60 14.80 15.00 15.20 267 m/z 356.10 12.34%| 5000 179 356 45 147 | , |, , 209 237 . 312 . —T000011111—0011—00—90009000100T012—0330003———210121111 nfe-> 40 60 80 100120140160180200220240260280300320340360380400420440 Abundance 73 #57357: Noradrenaline, tetra-TMS 1 14,40 14.60 14.80 15,00 15.20 m/z 267.95 9.33%

5000 102 355

45 147 442 TWTTTTTTTTTT i" " i i “' ■ ।" " i111111111 r111111111'111111111 __ ------------------ m/z—> 40 60 80 100120140160180200220240260280300320340360380400420440 14.40 14.60 14.80 15.00 15.20

8485.D GCMS0510.M Fri Mav 10 13:57:47 2002 Dana 2

NYC-WTC_000023281

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NYC-WTC_000023281Source: NYC Law Department, mirrored locally

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